ChemicalBook > CAS DataBase List > 2-Chloro-5-trichloromethylpyridine
2-Chloro-5-trichloromethylpyridine
2-Chloro-5-trichloromethylpyridine
- CAS No.69045-78-9
- Chemical Name:2-Chloro-5-trichloromethylpyridine
- CBNumber:CB8247348
- Molecular Formula:C6H3Cl4N
- Formula Weight:230.91
- MOL File:69045-78-9.mol
2-Chloro-5-trichloromethylpyridine Property
- Melting point -18.14 °C
- Boiling point 281.8±35.0 °C(Predicted)
- Density 1.582±0.06 g/cm3(Predicted)
- storage temp. under inert gas (nitrogen or Argon) at 2-8°C
- form solid
- pka -2.26±0.10(Predicted)
- color Pink
- CAS DataBase Reference 69045-78-9(CAS DataBase Reference)
- FDA UNII 7YHC64YM0S
- EPA Substance Registry System 2-Chloro-5-(trichloromethyl)pyridine (69045-78-9)
Safety
- Hazard Codes :Xi,T
- Risk Statements :36/37/38-25
- Safety Statements :26-37/39-45
- RIDADR :UN2811
- Hazard Note :Irritant
- HS Code :2933399990
-
Symbol(GHS)
- Signal wordWarning
- Hazard statements H302-H315-H319-H335
- Precautionary statements P260-P280-P312
2-Chloro-5-trichloromethylpyridine Chemical Properties,Usage,Production
- Synthesis A synthetic method of 2-chloro-5-trichloromethyl pyridine comprises the following steps of (1) synthesis of N-oxygen-3-methylpyridine: reacting by taking 3-methylpyridine as a raw material, glacial acetic acid as a solvent and 60% hydrogen peroxide as an oxidizing agent to obtain N-oxygen-3-methylpyridine; (2) synthesis of 2-chloro-5-methylpyridine: carrying out oriented chlorination on N-oxygen-3-methylpyridine by taking benzoyl chloride as a chlorinating agent to obtain 2-chloro-5-methylpyridine; (3) synthesis of 2-chloro-5-trichloromethyl pyridine: reacting by taking methyl ethyl ketone peroxide as an initiating agent to obtain a crude 2-chloro-5-trichloromethyl pyridine product; (4) refining of 2-chloro-5-trifluoromethyl pyridine: carrying out halogen exchange fluoridation reaction by taking excessive potassium fluoride as a fluorizating agent, dimethyl sulfoxide as a solvent and hexadecyl trimethyl ammonium bromide as a phase transfer catalyst, and rectifying and purifying to obtain a fine 2-chloro-5-trichloromethyl pyridine product.
2-Chloro-5-trichloromethylpyridine Preparation Products And Raw materials
Raw materials
Preparation Products
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69045-78-9, 2-Chloro-5-trichloromethylpyridineRelated Search:
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- Imidazoles
- Heterocycle-Pyridine series
- API Intermediate
- Pyridine
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- Halides
- 化工中间体
- 医用原料
- 高端化学
- 吡啶类
- 中间体-农药中间体
- 中间体
- 农药中间体
- C6H3CI4N
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- 69045-78-9
- 2-Chloro-5-trichloromethylpyridine ISO 9001:2015 REACH
- oro-5-trichL
- Pyridine, 2-chloro-5-(trichloromethyl)-
- 2-Chloro-5-trichloromethylpyridine###NA
- AKOS BBS-00000412
- 2-CHLORO-5-TRICHLOROMETHYL PYRIDINE
- IFLAB-BB F0797-0001