ChemicalBook > CAS DataBase List > 4-Methyl-3-nitrobenzoic acid methyl ester

4-Methyl-3-nitrobenzoic acid methyl ester

Synthesis

4-Methyl-3-nitrobenzoic acid methyl ester Property

Melting point 49-53°C
Boiling point 298.0±20.0 °C(Predicted)
Density 1?+-.0.06 g/cm3(Predicted)
Flash point 110 °C
storage temp. Sealed in dry,Room Temperature
solubility Soluble in methanol.
form powder to crystal
color White to Light yellow
CAS DataBase Reference 7356-11-8(CAS DataBase Reference)
FDA UNII SP3WQE4WRB
EPA Substance Registry System Benzoic acid, 4-methyl-3-nitro-, methyl ester (7356-11-8)
UNSPSC Code 12352100
NACRES NA.22

Safety

NFPA 704:

Hazard and Precautionary Statements (GHS)

4-Methyl-3-nitrobenzoic acid methyl ester Price More Price(6)

4-Methyl-3-nitrobenzoic acid methyl ester Chemical Properties,Usage,Production

Synthesis Methyl 4-methyl-3-nitrobenzoate is synthesized by the following steps:Acid 33 (100 g, 0.552 mol) was dissolved in MeOH (1000 ml). Conc. H2SO4 (30 ml) was added cautiously to this solution. The mixture was refluxed for 8 hours. Solvent was distilled off. Ice-cold water was added to the residue. It was then extracted with EtOAc, washed with NaHCO3 solution, water, dried (anhydrous Na2SO4), filtered and concentrated in vacuo to furnish faint yellow a solid. (91.57 g).
Chemical Properties White solid
Uses Methyl 4-methyl-3-nitrobenzoate is used as pharmaceutical intermediate.

4-Methyl-3-nitrobenzoic acid methyl ester Preparation Products And Raw materials

Raw materials

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4-Methyl-3-nitrobenzoic acid methyl ester Spectrum

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