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1-Bromo-4-(pentafluorosulfanyl)benzene

1-Bromo-4-(pentafluorosulfanyl)benzene Structure
1-Bromo-4-(pentafluorosulfanyl)benzene
  • CAS No.774-93-6
  • Chemical Name:1-Bromo-4-(pentafluorosulfanyl)benzene
  • CBNumber:CB5263002
  • Molecular Formula:C6H4BrF5S
  • Formula Weight:283.06
  • MOL File:774-93-6.mol
1-Bromo-4-(pentafluorosulfanyl)benzene Property
  • Boiling point 77.2 °C(Press: 10 Torr)
  • refractive index 1.4790-1.4830
  • Flash point 84°C(lit.)
  • storage temp. 0-10°C
  • form liquid
  • color Clear, colourless
  • InChI InChI=1S/C6H4BrF5S/c7-5-1-3-6(4-2-5)13(8,9,10,11)12/h1-4H
  • InChIKey RECCABBXFXGELM-UHFFFAOYSA-N
  • SMILES S(F)(F)(F)(F)(F)C1=CC=C(Br)C=C1
Safety
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal wordWarning
  • Hazard statements H227-H302-H315-H319
  • Precautionary statements P210-P264-P270-P280-P301+P312+P330-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313-P403+P235-P501
1-Bromo-4-(pentafluorosulfanyl)benzene Price More Price(1)
  • Brand: TCI Chemicals (India)
  • Product number: B3867
  • Product name : 4-Bromophenylsulfur Pentafluoride
  • Purity: min. 96.0 %
  • Packaging: 1G
  • Price: ₹9200
  • Updated: 2022/05/26
  • Buy: Buy

1-Bromo-4-(pentafluorosulfanyl)benzene Chemical Properties,Usage,Production

  • Synthesis 5.0 g of 4-pentafluorosulfanylaniline was dissolved in 20 ml of acetic acid, and, at 0 ℃, a saturated aqueous HBr solution was added. Then, at 0 ℃, a solution of 1.9 of NaNO2 in 5 ml of water was slowly added dropwise over the course of 5 minutes. The reaction mixture was stirred at 0 C. for 10 minutes and then added in portions to a suspension of 6.5 g of CuBr in 20 ml of a half-saturated aqueous HBr solution at 0 ℃. Nitrogen is liberated during this. The mixture was stirred at 0 ℃. for 30 minutes and then at RT for 1 h. It was subsequently extracted 3 times with 100 ml of HEP each time, and then the HEP was washed twice with 50 ml of a saturated aqueous Na2CO3 solution each time. The residue, after drying over MgSO4 and removal of the solvent in vacuo, was chromatographed on silica gel with HEP. 1.8 g of a colorless oil 1-Bromo-4-(pentafluorosulfanyl)benzene were obtained.
1-Bromo-4-(pentafluorosulfanyl)benzene Preparation Products And Raw materials
Raw materials
Preparation Products
1-Bromo-4-(pentafluorosulfanyl)benzene Suppliers
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1-Bromo-4-(pentafluorosulfanyl)benzene Spectrum
774-93-6, 1-Bromo-4-(pentafluorosulfanyl)benzeneRelated Search:
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  • Phenyls & Phenyl-Het
  • Halides
  • 亚磺酰胺
  • 磺胺类药物
  • C6H4F5BrS
  • (OC-6-21)-(4-溴苯基)五氟硫
  • 对溴苯基五氟化硫
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