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Methyl 2,4-dichloropyrimidine-6-carboxylate

Methyl 2,4-dichloropyrimidine-6-carboxylate Structure
Methyl 2,4-dichloropyrimidine-6-carboxylate
  • CAS No.6299-85-0
  • Chemical Name:Methyl 2,4-dichloropyrimidine-6-carboxylate
  • CBNumber:CB4326700
  • Molecular Formula:C6H4Cl2N2O2
  • Formula Weight:207.01
  • MOL File:6299-85-0.mol
Methyl 2,4-dichloropyrimidine-6-carboxylate Property
  • Melting point 54-56
  • Boiling point 306 ºC
  • Density 1.503
  • Flash point 139 ºC
  • storage temp. under inert gas (nitrogen or Argon) at 2-8°C
  • form White to off white to faint cream flakes
  • pka -5.83±0.30(Predicted)
Safety
  • Hazard Codes  :Xi
  • HazardClass  :IRRITANT
  • HS Code  :2933599590
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal wordWarning
  • Hazard statements H315-H319
  • Precautionary statements P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313

Methyl 2,4-dichloropyrimidine-6-carboxylate Chemical Properties,Usage,Production

  • Synthesis To a stirred suspension of orotic acid (20.00 g, 128.140 mmol) in POCI3(75 ml) was added DMF (catalytic amount, -0.5 ml) at ambient temperature, and the resulting reaction mixture was refluxed for 3 h. Excess of POC was removed by vacuum distillation after 3h of reflux. The obtained slurry was poured slowly into a 5 per cent mixture of methanol in chloroform (200 ml) at 0°C and stirred for 30 min. The organic layer obtained was washed with a saturated solution of NaHCC>3 (3 x 200 ml). The combined organic phase was dried over Na2S04, filtered and concentrated under reduced pressure, yielding Methyl 2,4-dichloropyrimidine-6-carboxylate (19.00 g, 91 .800 mmol).
Methyl 2,4-dichloropyrimidine-6-carboxylate Preparation Products And Raw materials
Raw materials
Preparation Products
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Methyl 2,4-dichloropyrimidine-6-carboxylate Spectrum
6299-85-0, Methyl 2,4-dichloropyrimidine-6-carboxylateRelated Search:
  • pharmacetical
  • Heterocycle-Pyrimidine series
  • 杂环化合物
  • 医用原料
  • 嘧啶
  • 外
  • 合成材料中间体
  • 医药中间体
  • 杂环
  • 药物中间体
  • 嘧啶系列
  • 6299-45-0
  • 甲基 2,6-二氯嘧啶-4-甲酸酯
  • 甲基 2,6-二氯嘧啶-4-甲酸基酯
  • N-(2-(4-硝基苯基)乙基)氨基甲酸叔丁酯
  • 2,4-二氯-6-嘧啶甲酸甲酯
  • 2,4-二氯嘧啶-6-羧酸甲酯
  • 2-甲基-4-氯-5-嘧啶甲酸甲酯
  • 2,4-二氯嘧啶-6-甲酸甲酯
  • 2,6-二氯嘧啶-4-甲酸甲酯
  • 6299-85-0
  • 2-(3-chlorophenyl)malondialdehyde,98%
  • 2,6-Dichloro-pyrimidine-4-carboxylic acid methyl ester
  • Methyl 2,6-dichloropyrimidine-4-carboxylate
  • 6-c
  • Tert-butyl n-(2-(4-nitrophenyl)ethyl)carbamate
  • 2,4-dichloropyrimidine-6-carboxylate
  • 4-PyriMidinecarboxylicacid, 2,6-dichloro-, Methyl ester
  • Methyl 2,4-dichloropyrimidine-6-carboxylate
  • 4-Methyl-2-(3,4-dichlorophenyl)thiazole-5-carboxylicacid
  • 2-(3-CHLOROPHENYL)MALONDIALDEHYDE
  • Methyl2,4-dichloropyrimidine-6-carboxylate99%
  • Methyl 2,4-dichloropyrimidine-6-carboxylate 99%
  • NSC45044
  • 2,6-DICHLORO-PYRIMIDINE-4-CARBOXYLIC ACID ETHYL ESTER
  • 2,6-dichloropyrimidine-4-carboxylate
  • 2,4-Dichloro-6-(methoxycarbonyl)pyrimidine

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