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Ethyl 3-Amino-4-methylbenzoate

Ethyl 3-Amino-4-methylbenzoate Structure
Ethyl 3-Amino-4-methylbenzoate
  • CAS No.41191-92-8
  • Chemical Name:Ethyl 3-Amino-4-methylbenzoate
  • CBNumber:CB3823116
  • Molecular Formula:C10H13NO2
  • Formula Weight:179.22
  • MOL File:41191-92-8.mol
Ethyl 3-Amino-4-methylbenzoate Property
  • Melting point 48.6-50.1℃
  • Boiling point 105°C/0.2mmHg(lit.)
  • Density 1.103±0.06 g/cm3(Predicted)
  • storage temp. under inert gas (nitrogen or Argon) at 2–8 °C
  • solubility soluble in Methanol
  • form powder to crystal
  • pka 3.35±0.10(Predicted)
  • color White to Almost white
  • InChIKey MCNBNDUVWQEKNZ-UHFFFAOYSA-N
Safety
  • HS Code  :2922498590
  • NFPA 704:
    0
    1 0
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal wordWarning
  • Hazard statements H315-H319
  • Precautionary statements P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313
Ethyl 3-Amino-4-methylbenzoate Price More Price(1)
  • Brand: TCI Chemicals (India)
  • Product number: E1025
  • Product name : Ethyl 3-Amino-4-methylbenzoate
  • Purity: min. 98.0 %
  • Packaging: 5G
  • Price: ₹7600
  • Updated: 2022/05/26
  • Buy: Buy

Ethyl 3-Amino-4-methylbenzoate Chemical Properties,Usage,Production

  • Synthesis Dissolve 10 g of palladium on carbon (10%) and 140 g of ammonium formate in 400 ml of methanol, and then dissolve 136 g of ethyl 3-nitro-4-methylbenzoate (2) in 400 ml of methanol. Add the methanol solution of (2) dropwise to the reaction flask at room temperature. The reaction exotherms until the methanol boils. Continue the dropwise addition. After the dropwise addition, TLC detects the completion of the reaction and filters the palladium carbon. Concentrate the methanol, add 400ml of water, and filter to obtain 156g of white solid ethyl 3-amino-4-methylbenzoate (Ethyl 3-Amino-4-methylbenzoate) as a wet product, which can be used in the next step without drying.
    Ethyl 3-Amino-4-methylbenzoate
Ethyl 3-Amino-4-methylbenzoate Preparation Products And Raw materials
Raw materials
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Ethyl 3-Amino-4-methylbenzoate Spectrum
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