ChemicalBook > CAS DataBase List > 5-Amino-7-azaindole
5-Amino-7-azaindole
5-Amino-7-azaindole
- CAS No.100960-07-4
- Chemical Name:5-Amino-7-azaindole
- CBNumber:CB3375549
- Molecular Formula:C7H7N3
- Formula Weight:133.15
- MOL File:100960-07-4.mol
5-Amino-7-azaindole Property
- Melting point 128-129°C
- Boiling point 361.7±35.0 °C(Predicted)
- Density 1.41±0.1 g/cm3(Predicted)
- storage temp. Keep in dark place,Sealed in dry,Room Temperature
- pka 8.28±0.20(Predicted)
- form Solid
- color Yellow to yellow/brown
- Sensitive Light Sensitive
- InChIKey PLWBENCHEUFMTN-UHFFFAOYSA-N
- CAS DataBase Reference 100960-07-4
- UNSPSC Code 12352116
Safety
-
Symbol(GHS)
- Signal wordWarning
- Hazard statements H302-H319
- Precautionary statements P264-P270-P280-P301+P312-P305+P351+P338-P337+P313
5-Amino-7-azaindole Price
More Price(1)
- Brand: Sigma-Aldrich(India)
- Product number: ADE000889
- Product name : 1H-Pyrrolo[2,3-b]pyridin-5-ylamine
- Purity: AldrichCPR
- Packaging: 1G
- Price: ₹68706.28
- Updated: 2022/06/14
- Buy: Buy
5-Amino-7-azaindole Chemical Properties,Usage,Production
- Chemical Properties Brown crystalline powder
-
Synthesis
5-Amino-7-azaindole is synthesised using 5-Nitro-7-azaindole as a raw material by chemical reaction. The specific synthesis steps are as follows:
To a stirred solution of 5nitro7azaindoie (500 rng, 3.07 rnmol) in methanol (125 rnL) under nitrogen atmosphere was added 10percent Pd/C (326 mg, 0.306 rnmol). The reaction was placed under an atmosphere of hydrogen gas and stirred at 20 °C overnight. The suspension was filtered through a pad of Celite? 545, the resulting filter cake was washed with MeOH, and the combined organicphases concentrated in vaeuo to afford 5-Amino-7-azaindole compound (408 mg, 100percent). MS (ES1): mass calcd. for C7HN3 133.1, rn/z found 133.9 [M+H]t. ‘H NMR (300 MHz, DMSO-d6) ? 11.04 (s, 1H), 7.70 (d, J= 2.4 Hz, iH, 7.27 —7.18 (m, 1ff), 7.08 (d, J= 2.3 Hz, IH), 6.22 —6.06 (m, 1H), 4.62 (s, 2H).
5-Amino-7-azaindole Preparation Products And Raw materials
Raw materials
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100960-07-4, 5-Amino-7-azaindoleRelated Search:
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