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4-Chloro-2-fluorobenzyl alcohol

4-Chloro-2-fluorobenzyl alcohol Structure
4-Chloro-2-fluorobenzyl alcohol
  • CAS No.56456-49-6
  • Chemical Name:4-Chloro-2-fluorobenzyl alcohol
  • CBNumber:CB0676047
  • Molecular Formula:C7H6ClFO
  • Formula Weight:160.57
  • MOL File:56456-49-6.mol
4-Chloro-2-fluorobenzyl alcohol Property
  • Boiling point 227.6±25.0 °C(Predicted)
  • Density 1.344±0.06 g/cm3(Predicted)
  • storage temp. Sealed in dry,Room Temperature
  • pka 13.68±0.10(Predicted)
  • CAS DataBase Reference 56456-49-6(CAS DataBase Reference)
Safety
  • Hazard Codes  :Xi
  • Risk Statements  :36/37/38
  • Safety Statements  :26-36/37/39
  • HazardClass  :IRRITANT
  • HS Code  :2906290090
Hazard and Precautionary Statements (GHS)
  • Symbol(GHS)
  • Signal wordWarning
  • Hazard statements H315-H319-H335
  • Precautionary statements P261-P305+P351+P338

4-Chloro-2-fluorobenzyl alcohol Chemical Properties,Usage,Production

  • Synthesis A solution of 4-chloro-2-fluorobenzoic acid (300mg) in THF (15m1) was added at 0CLiAIH4 (130mg). The suspension was stirred at 0℃ for 16h. The reaction mixture was diluted with EA and aq. A solution of potassium sodium tartrate was stirred for lh at rt. The layers were separated, and the org. phasel was further washed with water. The combined org. layers were dried over MgSO4, filtrated off and evaporated in vacuo. The crude was purified by CC (Buechi Sepacore, 5g cartridge, solvent A: DCM, solvent B: 3N ammonia in MeOH, gradient in %B: 0 to 5, flow rate: 6.0 mI/mm) to afford 224mg of colourless oil 4-Chloro-2-fluorobenzyl alcohol. LCMS: (A) tR = 0.68 mm; [M+H]: not visible.
4-Chloro-2-fluorobenzyl alcohol Preparation Products And Raw materials
Raw materials
Preparation Products
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4-Chloro-2-fluorobenzyl alcohol Spectrum
56456-49-6, 4-Chloro-2-fluorobenzyl alcoholRelated Search:
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  • RARECHEM AL BD 0387

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