1,2-Difluor-3-nitrobenzol

Gefahreninformationscode (GHS)

• Bildanzeige (GHS)

  

• Alarmwort

  Warnung

• Gefahrenhinweise

  H315：Verursacht Hautreizungen.

  H319：Verursacht schwere Augenreizung.

  H335：Kann die Atemwege reizen.

• Sicherheit

  P261：Einatmen von Staub vermeiden.

  P305+P351+P338：BEI KONTAKT MIT DEN AUGEN: Einige Minuten lang behutsam mit Wasser spülen. Eventuell vorhandene Kontaktlinsen nach Möglichkeit entfernen. Weiter spülen.

2,3-Difluoronitrobenzene Chemische Eigenschaften,Einsatz,Produktion Methoden

• Chemische Eigenschaften

  Light yellow transparent liquid

• Synthese

  To a stirred solution of hydroxy peroxide (30 % in H2O, 35 mL, 356 mmol) under N2 at 0℃, a solution of trifluoroacetic anhydride (56 mL, 407 mmol) in 115 mL dichloromethane was added dropwise over 2 h. After the addition was complete, a solution of 2,3- difluorobenzenamine (5 g, 39 mmol) in 115 mL dichloromethane was added dropwise at 0℃. After the addition was complete, the reaction mixture was gradually warmed to room temperature and stirred overnight. The mixture was extracted by dichloromethane and dried over anhydrous Na2SO4. The mixture was filtered and concentrated under reduced pressure. The residue was purified by flash column with 0-15 % EtOAc in hexane to yield 3.5 g of 2,3-Difluoronitrobenzene (57%).

1,2-Difluor-3-nitrobenzol Anbieter Lieferant Produzent Hersteller Vertrieb Händler.

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