29182-96-5

0.05g of solid 3-nitro aniline was weighed on  weighing balance and then transferred to a clean iodine flask of 250 ml in which 10 ml  solution of 10% sodium carbonate was already  present. Mix the reaction mixture so that solid aniline  got dissolved in Na2CO3 solution evenly. After that  bromoacetyl bromide was added gradually and shaken  vigorously for 10 minutes to prepare solid precipitates  which were filtered later with proper washing. Solid  precipitates were collected, weighed and saved.