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• Synthesis

  

  In a 10 mL sealed tube, p-cresol (1.2 mmol), cuprous iodide (0.05 mmol), ligand L-II-34 (0.1 mmol), and potassium phosphate (2.0 mmol) were added. The tube was purged with argon three times under vacuum. Then, p-methylchlorobenzene (1.0 mmol) and 1 mL DMSO were added. The reaction was stirred uniformly at 120 °C for 24 hours. After cooling, the contents of the sealed tube were washed with ethyl acetate and filtered through a silica gel and diatomaceous earth column. The filtrate was concentrated and then subjected to column chromatography to obtain the product 4-Tolyl ether.

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