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网站主页CAS数据库列表 5472-49-1更多图谱N-(3-氯丙基)哌啶盐酸盐(5472-49-1)核磁图(13CNMR)

N-(3-氯丙基)哌啶盐酸盐

产品名称 N-(3-氯丙基)哌啶盐酸盐

CAS号5472-49-1

分子式C8H17Cl2N

分子量198.13


  • Mass

    MS-IW-6293          
    1-(3-chloropropyl)piperidine hydrochloride
    C8H16ClN HCl        (Mass of molecular ion:    161)
    

       Source Temperature: 150 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          27.0       1.0
          28.0       1.4
          30.0       1.2
          36.0       9.7
          38.0       3.2
          39.0       1.3
          41.0       5.5
          42.0       5.6
          43.0       1.9
          44.0       2.8
          55.0       5.7
          56.0       1.4
          69.0       2.4
          70.0       3.5
          84.0       1.4
          96.0       1.3
          98.0     100.0
          99.0       7.2
         160.0       3.7
         161.0       7.3
         162.0       1.9
         163.0       2.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H16 Cl N 0.046 g : 0.5 ml CDCl3
    1-(3-chloropropyl)piperidine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.697 B 3.544 C 3.188 D 2.843 E 2.467 F 2.24 G 1.895 J 1.50

         Hz     ppm     Int.
    

       1483.52   3.713    814
       1477.54   3.698   1000
       1474.49   3.690    141
       1471.56   3.683    813
       1420.53   3.555    304
       1408.94   3.526    311
       1280.40   3.204    247
       1275.15   3.191    300
       1274.54   3.190    300
       1268.43   3.174    251
       1152.47   2.884    115
       1142.33   2.859    218
       1132.81   2.835    212
       1121.70   2.807    101
        998.66   2.499    197
        992.55   2.484    314
        990.60   2.479    218
        989.26   2.476    207
        986.69   2.469    337
        984.50   2.464    296
        982.42   2.459    343
        976.07   2.443    268
        970.34   2.428    154
        917.60   2.297     88
        914.06   2.288     80
        905.03   2.265    208
        902.95   2.260    199
        893.43   2.236    198
        890.26   2.228    224
        881.10   2.205     87
        877.69   2.197    101
        874.51   2.189     67
        762.82   1.909    495
        751.71   1.881    436
        616.58   1.543     61
        613.28   1.535     54
        605.22   1.515    113
        603.76   1.511    119
        600.71   1.504    113
        594.36   1.488     92
        591.19   1.480    107
    

in CDCl3



KBr disc



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