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网站主页CAS数据库列表 5407-04-5更多图谱N,N-二甲氨基氯丙烷盐酸盐(5407-04-5)红外图谱(IR2)

N,N-二甲氨基氯丙烷盐酸盐

产品名称 N,N-二甲氨基氯丙烷盐酸盐

CAS号5407-04-5

分子式C5H13Cl2N

分子量158.07

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  • Mass

    MS-NW-6312          
    3-chloro-N,N-dimethylpropylamine hydrochloride
    C5H12ClN HCl        (Mass of molecular ion:    121)
    

       Source Temperature: 180 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          15.0       4.0
          18.0       1.3
          27.0       2.1
          28.0       2.0
          29.0       1.6
          30.0       5.3
          35.0       2.1
          36.0      15.5
          38.0       5.1
          39.0       2.0
          41.0       3.3
          42.0       9.8
          43.0       2.4
          44.0       5.4
          56.0       1.8
          57.0       1.9
          58.0     100.0
          59.0       4.0
          70.0       1.2
          71.0       1.5
          84.0       1.7
          85.0       1.2
         121.0       4.9
         123.0       1.7
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C5 H12 Cl N 0.047 g : 0.5 ml CDCl3
    3-chloro-N,N-dimethylpropylamine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.739 B 3.52 C 3.319 D 2.931 E 2.385

         Hz     ppm     Int.
    

       1500.49   3.755    203
       1494.38   3.740    272
       1488.16   3.724    196
       1407.35   3.522    164
       1336.67   3.345     75
       1331.30   3.332    107
       1328.86   3.326     80
       1325.44   3.317     75
       1323.49   3.312     80
       1320.80   3.305    103
       1315.43   3.292     72
       1182.50   2.959     34
       1173.71   2.937   1000
       1168.70   2.925    927
        966.92   2.420     49
        960.82   2.405     89
        959.23   2.401     62
        956.67   2.394     60
        954.83   2.390     88
        952.88   2.385     85
        950.93   2.380     91
        944.82   2.365     81
        938.84   2.350     42
    


  • 1H NMR 89.56 MHz
    C5 H12 Cl N 0.047 g : 0.5 ml CDCl3
    3-chloro-N,N-dimethylpropylamine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 11.9 B 3.734 C 3.33 D 2.923 E 2.39 J(A,D)=5.0HZ.

         Hz     ppm     Int.
    

        340.77   3.805    156
        334.79   3.739    247
        328.64   3.670    193
        307.36   3.432     56
        304.28   3.398    160
        302.58   3.379     90
        300.27   3.353     65
        295.48   3.300     64
        291.81   3.259     96
        286.51   3.200     75
        264.29   2.951   1000
        259.25   2.895    988
        227.29   2.538     36
        226.95   2.535     36
        220.89   2.467     74
        219.09   2.447     47
        218.58   2.441     47
        216.02   2.413     54
        214.90   2.400     63
        212.94   2.378     60
        211.32   2.360     74
        206.02   2.301     51
        204.99   2.289     52
    

in CDCl3



KBr disc



liquid film



nujol mull



4880 A,200 M,powder