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网站主页CAS数据库列表 5394-18-3更多图谱N-(4-溴丁基)邻苯二甲酰亚胺(5394-18-3)核磁图(13CNMR)

N-(4-溴丁基)邻苯二甲酰亚胺

产品名称 N-(4-溴丁基)邻苯二甲酰亚胺

CAS号5394-18-3

分子式C12H12BrNO2

分子量282.13


  • Mass

    MS-NW-8793          
    N-(4-bromobutyl)phthalimide
    C12H12BrNO2         (Mass of molecular ion:    281)
    

       Source Temperature: 170 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       1.0
          27.0       1.8
          28.0       1.0
          39.0       1.4
          41.0       1.8
          50.0       4.0
          51.0       2.3
          53.0       1.0
          55.0       1.6
          74.0       1.2
          75.0       2.7
          76.0      10.0
          77.0       9.2
         102.0       2.2
         103.0       1.2
         104.0       8.3
         105.0       6.6
         130.0       7.7
         132.0       1.2
         133.0       4.9
         147.0       1.2
         148.0       3.4
         160.0     100.0
         161.0      10.7
         174.0       4.9
         175.0       1.1
         188.0       2.0
         201.0      12.0
         202.0      47.3
         203.0       6.4
         281.0       3.7
         283.0       3.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H12 Br N O2 0.036 g : 0.5 ml CDCl3
    N-(4-bromobutyl)phthalimide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.849 B 7.730 C 3.731 D 3.451 E 1.90 F 1.86

         Hz     ppm     Int.
    

       3147.22   7.875     36
       3145.75   7.872     53
       3141.97   7.862    719
       3138.92   7.855    715
       3136.35   7.848    556
       3133.42   7.841    977
       3130.25   7.833     60
       3129.52   7.831    116
       3128.30   7.828    103
       3098.39   7.753     81
       3097.17   7.750    102
       3095.95   7.747     37
       3093.38   7.741    901
       3090.33   7.733    559
       3087.89   7.727    684
       3084.84   7.719    713
       3081.05   7.710     85
       3079.59   7.706     55
       1497.80   3.748    459
       1490.97   3.731    878
       1484.25   3.714    381
       1385.99   3.469    398
       1379.64   3.453   1000
       1373.17   3.436    522
        780.52   1.954     42
        778.44   1.948     44
        773.93   1.937    100
        771.61   1.931    129
        768.55   1.924    128
        766.36   1.918    140
        765.14   1.915    237
        762.57   1.909    181
        761.96   1.907    164
        758.91   1.899    301
        757.69   1.896    278
        755.37   1.891    230
        754.39   1.888    231
        753.30   1.885    224
        752.20   1.883    234
        749.76   1.877    265
        748.41   1.873    283
        744.87   1.864    189
        742.92   1.859    199
        742.07   1.857    219
        741.09   1.855    166
        738.53   1.848    119
        735.60   1.841    127
        733.15   1.835    122
        728.64   1.824     49
        726.44   1.818     47
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder