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3-硝基邻苯二甲酰亚胺

产品名称 3-硝基邻苯二甲酰亚胺

CAS号603-62-3

分子式C8H4N2O4

分子量192.13

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  • Mass

    MS-NW-6436          
    3-nitrophthalimide
    C8H4N2O4            (Mass of molecular ion:    192)
    

       Source Temperature: 140 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          17.0       2.7
          18.0      13.6
          28.0       4.9
          30.0      21.3
          37.0       4.1
          38.0       2.7
          39.0       2.0
          43.0       1.1
          44.0       1.5
          49.0       1.9
          50.0       2.0
          51.0       1.2
          52.0       1.0
          53.0       1.0
          61.0       2.0
          62.0       3.6
          63.0       5.0
          64.0       1.4
          65.0       1.1
          70.0       1.4
          73.0       2.9
          74.0      19.4
          75.0     100.0
          76.0       7.8
          77.0       1.2
          78.0       1.4
          89.0       1.9
          90.0       2.5
          91.0       5.4
         102.0       5.4
         103.0      60.8
         104.0       4.9
         105.0       1.7
         106.0       3.2
         118.0       1.0
         119.0       9.9
         120.0       1.0
         146.0       8.2
         148.0       3.1
         149.0       4.9
         162.0      14.2
         163.0       1.9
         176.0       1.3
         192.0      73.8
         193.0       7.4
         194.0       1.0
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C8 H4 N2 O4 0.040 g : 0.5 ml DMSO-d6
    3-nitrophthalimide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 11.8 B 8.268 C 8.127 D 8.057

         Hz     ppm     Int.
    

       4713.05  11.793    159
       3309.27   8.281    643
       3308.35   8.279    790
       3305.24   8.271     43
       3304.32   8.269     42
       3301.39   8.261    797
       3300.29   8.258    823
       3253.40   8.141    488
       3252.49   8.139    693
       3249.19   8.131     47
       3245.89   8.122    900
       3244.98   8.120   1000
       3227.21   8.076    870
       3223.55   8.066     35
       3223.00   8.065     35
       3219.70   8.057    748
       3219.33   8.056    964
       3215.12   8.045     36
       3211.82   8.037    525
    

in DMSO-d6



KBr disc



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