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网站主页CAS数据库列表 116325-74-7更多图谱2,2-双(3-氨基-4-甲苯基)六氟丙烷(116325-74-7)质谱(MS)

2,2-双(3-氨基-4-甲苯基)六氟丙烷

产品名称 2,2-双(3-氨基-4-甲苯基)六氟丙烷

CAS号116325-74-7

分子式C17H16F6N2

分子量362.31

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  • Mass

    MS-IW-1777          
    5,5'-(hexafluoroisopropylidene)bis(o-toluidine)
    C17H16F6N2          (Mass of molecular ion:    362)
    

       Source Temperature: 160 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          77.0       1.1
         104.0       4.3
         104.5       5.1
         111.0       1.0
         112.0       2.0
         129.0       1.2
         131.5       2.3
         138.5       1.7
         139.0       7.5
         139.5       1.2
         146.5       1.0
         166.0       2.7
         173.0       1.0
         173.5       1.8
         180.0       1.3
         181.0       5.0
         207.0       1.9
         208.0       2.7
         209.0       7.2
         210.0       1.3
         211.0       1.1
         223.0       2.3
         224.0       1.3
         258.0       1.2
         263.0       1.9
         275.0       1.8
         276.0       5.4
         277.0       6.5
         278.0      26.9
         279.0       4.6
         291.0       1.5
         292.0       1.8
         293.0      12.1
         294.0       2.2
         323.0       2.2
         331.0       1.3
         332.0       4.8
         333.0       1.0
         344.0       1.1
         345.0       2.6
         346.0       9.9
         347.0       7.3
         348.0       1.2
         361.0       9.9
         362.0     100.0
         363.0      19.3
         364.0       1.8
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C17 H16 F6 N2 0.032 g : 0.5 ml DMSO-d6
    5,5'-(hexafluoroisopropylidene)bis(o-toluidine)
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.956 B 6.616 C 6.465 D 5.01 E 2.046

         Hz     ppm     Int.
    

       2783.94   6.966    172
       2775.51   6.945    185
       2644.04   6.616    189
       2587.65   6.475     98
       2579.83   6.456     92
       2001.10   5.008    377
        817.87   2.047   1000
        808.35   2.023     22
        807.37   2.021     22
        807.13   2.020     22
    

in DMSO-d6



KBr disc



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