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网站主页CAS数据库列表 47250-53-3更多图谱2,2-双(3-氨基苯基)六氟丙烷(47250-53-3)核磁图(13CNMR)

2,2-双(3-氨基苯基)六氟丙烷

产品名称 2,2-双(3-氨基苯基)六氟丙烷

CAS号47250-53-3

分子式C15H12F6N2

分子量334.26

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  • Mass

    MS-IW-7557          
    3,3'-(hexafluoroisopropylidene)dianiline
    C15H12F6N2          (Mass of molecular ion:    334)
    

       Source Temperature: 130 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       2.2
          28.0       1.1
          39.0       1.7
          65.0       2.6
          83.5       3.4
          84.0       1.4
          89.5       1.0
          97.5      10.7
          98.0      14.9
          98.5       2.2
          99.0       1.1
         108.5       1.1
         122.0       2.7
         122.5       2.5
         132.0       3.8
         132.5       5.2
         151.0       1.1
         152.0       1.7
         167.0       6.6
         168.0       1.9
         178.0       1.2
         179.0       1.7
         180.0       5.3
         181.0       1.1
         183.0       1.4
         195.0      15.0
         196.0       8.5
         197.0       1.2
         198.0       4.5
         201.0       1.1
         220.0       1.0
         225.0       3.4
         226.0       1.8
         228.0       1.0
         229.0       2.1
         244.0       3.7
         245.0       3.7
         246.0       1.0
         247.0       1.4
         248.0       8.7
         249.0       8.2
         250.0       1.6
         263.0       3.8
         264.0       8.4
         265.0      31.8
         266.0       5.3
         295.0       2.7
         316.0       2.1
         317.0       4.0
         318.0       3.1
         319.0       1.2
         333.0      19.0
         334.0     100.0
         335.0      16.8
         336.0       1.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15 H12 F6 N2 0.040 g : 0.5 ml CDCl3
    3,3'-(hexafluoroisopropylidene)dianiline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.122 B 6.814 C 6.68 D 6.666 E 3.61

         Hz     ppm     Int.
    

       2855.59   7.146    309
       2854.74   7.144    215
       2852.05   7.137     48
       2847.29   7.125    608
       2842.90   7.114     48
       2839.84   7.106    321
       2839.23   7.105    403
       2727.29   6.825    298
       2726.56   6.823    306
       2718.75   6.803    275
       2674.32   6.692    282
       2673.46   6.690    316
       2672.12   6.687    449
       2671.26   6.684    446
       2664.43   6.667    967
       2663.70   6.666   1000
       2653.81   6.641     25
       2652.47   6.637     22
       1442.26   3.609    120
    

in CDCl3



KBr disc



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