乙腈中22种氨基甲酸酯类农药混标
| CAS号 |
名称 |
标准值 |
单位 |
| 30614-22-3 |
脱甲基抗蚜威 |
100 |
μg/mL |
| 1646-87-3 |
涕灭威亚砜 |
100 |
μg/mL |
| 1646-88-4 |
涕灭威砜 |
100 |
μg/mL |
| 23103-98-2 |
抗蚜威 |
100 |
μg/mL |
| 16752-77-5 |
灭多威 |
100 |
μg/mL |
| 2635-10-1 |
甲硫威亚砜 |
100 |
μg/mL |
| 16655-82-6 |
3-羟基呋喃丹 |
100 |
μg/mL |
| 2179-25-1 |
甲硫威砜 |
100 |
μg/mL |
| 116-06-3 |
涕灭威 |
100 |
μg/mL |
| 1129-41-5 |
速灭威 |
100 |
μg/mL |
| 114-26-1 |
残杀威 |
100 |
μg/mL |
| 22781-23-3 |
恶虫威 |
100 |
μg/mL |
| 1563-66-2 |
克百威 |
100 |
μg/mL |
| 63-25-2 |
甲萘威 |
100 |
μg/mL |
| 2655-14-3 |
灭除威 |
100 |
μg/mL |
| 29973-13-5 |
杀虫丹 |
100 |
μg/mL |
| 2631-40-5 |
异丙威 |
100 |
μg/mL |
| 2686-99-9 |
3,4,5-混杀威 |
100 |
μg/mL |
| 3766-81-2 |
仲丁威 |
100 |
μg/mL |
| 2032-65-7 |
甲硫威 |
100 |
μg/mL |
| 72490-01-8 |
苯氧威 |
100 |
μg/mL |
| 144171-61-9 |
茚虫威 |
100 |
μg/mL |
备注：经与全国兽药残留专家委员会办公室确认，国标中氯灭杀威CAS号错误，改为涕灭威（116-06-3）
Reference Material
This certificate is designed in accordance with ISO 17034 and
ISO Guide 31. This reference material
(RM) was designed,produced and verified in accordance with ISO/IEC
17025, ISO 17034 and a registered
quality management system ISO 9001.
Product Name(产品名称)
22 Carbamate Pesticide Mix in Acetonitrile,100μg/mL(乙腈中22种氨基甲酸酯类农药混标)
Part Number(产品编号)
81882a
Lot Number(产品批号)
-
Expiry Date(失效日期)
2025-Feb-08____________________________
Storage(存储条件)
(-18±5)℃
冷冻(-18±5)℃
| CERTIFIED |
Component
No.
(组分数)
|
Peak
Sequence
(出峰顺序)
|
Component
(组分)
|
CAS No. |
Concentration
(μg/mL)
(浓度)
|
Relative Expanded
Uncertainty(%)
(k=2)
(相对扩展不确定度)
|
| 1 |
1 |
Desmethyl-pirimicarb
(脱甲基抗蚜威)
|
30614-22-3 |
100 |
3 |
| 2 |
2 |
Aldicarb-sulfoxide
(涕灭威亚砜)
|
1646-87-3 |
100 |
3 |
| 3 |
3 |
Aldicarb-sulfone
(涕灭威砜)
|
1646-88-4 |
100 |
3 |
| 4 |
4 |
Methomyl
(灭多威)
|
16752-77-5 |
100 |
3 |
| 5 |
5 |
Methiocarb-sulfoxide
(甲硫威亚砜)
|
2635-10-1 |
100 |
3 |
| 6 |
6 |
Pirimicarb
(抗蚜威)
|
23103-98-2 |
100 |
3 |
| 7 |
7 |
Carbofuran-3-hydroxy
(3-羟基呋喃丹)
|
16655-82-6 |
100 |
3 |
| 8 |
8 |
Methiocarb Sulfonein Acetone
(甲硫威砜)
|
2179-25-1 |
100 |
3 |
| 9 |
9 |
Aldicarb
(涕灭威)
|
116-06-3 |
100 |
3 |
| 10 |
10 |
Metolcarb
(速灭威)
|
1129-41-5 |
100 |
3 |
| 11 |
11 |
Propoxur
(残杀威)
|
114-26-1 |
100 |
3 |
| 12 |
12 |
Bendiocarb
(恶虫威)
|
22781-23-3 |
100 |
3 |
| 13 |
13 |
Carbofuran
(克百威)
|
1563-66-2 |
100 |
3 |
| 14 |
14 |
Carbaryl
(甲萘威)
|
63-25-2 |
100 |
3 |
| 15 |
15 |
XMC
(灭除威)
|
2655-14-3 |
100 |
3 |
| 16 |
16 |
Ethiofencarb
(杀虫丹)
|
29973-13-5 |
100 |
3 |
| 17 |
17 |
Isoprocarb
(异丙威)
|
2631-40-5 |
100 |
3 |
| 18 |
3,4,5-Trimethacarb
(3,4,5-混杀威)
|
2686-99-9 |
100 |
3 |
| 19 |
18 |
Fenobucarb
(仲丁威)
|
3766-81-2 |
100 |
3 |
| 20 |
19 |
Methiocarb
(甲硫威)
|
2032-65-7 |
100 |
3 |
| 21 |
20 |
Fenoxycarb
(苯氧威)
|
72490-01-8 |
100 |
3 |
| 22 |
21 |
Indoxacarb
(茚虫威)
|
144171-61-9 |
100 |
3 |
Instrument(检测仪器)
HPLC/MS-MS
Column(色谱柱)
C18(2.1x50mm,1.8μm)
Method Details(方法参数)
A：0.1% Formic Acid(0.1% 甲酸)
B：Acetonitrile(乙腈)
| Time/min |
A/% |
B/% |
| 0.00 |
70 |
30 |
| 2.00 |
70 |
30 |
| 7.00 |
10 |
90 |
| 9.00 |
10 |
90 |
| 10.00 |
70 |
30 |
Note
See the attachment below for the MRM mode.( 关于MRM模式，请参阅下面的附件。)
Intended Use
This RM is intended for use in a laboratory as a calibration and quality control standard or in
method development for analytical techniques.
Uncertainty
The certified value(s) and uncertainty(ies) are determined in accordance with ISO
17034 with an 95%
confidence level (k=2). Uncertainty is based on the Total Combined Uncertainty, including
uncertainties of preparation, purity of neat materials, homogeneity, stability testing.
Traceability
The balances used for gravimetric measurements are calibrated with weights traceable to the national
standards. The calibration of the balances is verified annually by an external accredited
calibration service. This analysis method has been verified using an approach consistent with
ISO 17034:2016 & ISO 17025:2017.
Homogeneity
Random replicate samples of the final packaged RM have been analysed to prove homogeneity consistent
with ISO 17034.
Storage
The RM should be stored in the original sealed bottle at the indicated temperature.
| CERTIFICATE ON |
QC SIGNATURE |
|
| - |
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|
RM Release |
标准品/乙腈中22种氨基甲酸酯类农药混标/GB 31658.10-2021;标准品/乙腈中22种氨基甲酸酯类农药混标/GB 31658.10-2021价格;标准品/乙腈中22种氨基甲酸酯类农药混标/GB 31658.10-2021厂家;TMstandard
