52230-29-2

4-三乙基磷钯

灰色结晶，低熔点固体

Experimental Procedure：
Hydrazine hydrate (20 mL) was added dropwise to a mixture of PdCl2 (0.44 g, 2.5 mM), ligand (PCy3, PEt3, or PMe3) (12.5 mM) in toluene (35 mL) at 120 °C. The light yellow mixture was stirred for 30 min at 120 °C and then cooled to room temperature. mononuclear aryl palladium(II) complex Pd(PR3)4. R=Et.

HNMR