图谱信息 供应商 相关产品
网站主页CAS数据库列表 94-99-5更多图谱2,4-二氯氯苄(94-99-5)Raman光谱

2,4-二氯氯苄

产品名称 2,4-二氯氯苄

CAS号94-99-5

分子式C7H5Cl3

分子量195.47

展开


  • Mass

    MS-NW-4683          
    alpha,2,4-trichlorotoluene
    C7H5Cl3             (Mass of molecular ion:    194)
    

       Source Temperature: 260 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          36.0       2.4
          37.0       1.5
          38.0       1.4
          39.0       3.3
          43.0       2.7
          43.5       1.0
          44.0       2.1
          49.0       1.2
          50.0       2.8
          51.0       1.6
          60.0       1.2
          61.0       6.7
          61.5       2.0
          62.0       6.8
          63.0       8.6
          73.0       5.6
          74.0       1.5
          75.0       2.3
          79.0       3.2
          79.5       1.2
          80.0       2.0
          85.0       1.7
          86.0       2.1
          87.0       2.7
          88.0       1.1
          89.0      11.6
          97.0       3.2
          99.0       2.9
         123.0      12.2
         124.0       5.2
         125.0       5.0
         126.0       1.7
         133.0       2.6
         135.0       1.6
         158.0       1.1
         159.0     100.0
         160.0       8.3
         161.0      61.7
         162.0       5.2
         163.0      10.2
         193.0       3.0
         194.0      16.8
         195.0       4.2
         196.0      15.9
         197.0       2.1
         198.0       5.2
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H5 Cl3 0.02 ml : 0.5 ml CDCl3
    alpha,2,4-trichlorotoluene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.648 B 7.264 C 7.38 D 7.41

         Hz     ppm     Int.
    

        667.75   7.456    104
        667.31   7.451     92
        664.50   7.420    202
        662.63   7.399    267
        659.44   7.364    334
        657.69   7.344     35
        653.19   7.294    289
        651.31   7.273    211
        644.94   7.202     83
        642.94   7.179     71
        416.31   4.649   1000
    

in CDCl3



CCl4 solution



liquid film



4880 A,200 M,liquid