图谱信息 供应商 相关产品
网站主页CAS数据库列表 89-95-2更多图谱邻甲基苄醇(89-95-2)Raman光谱

邻甲基苄醇

产品名称 邻甲基苄醇

CAS号89-95-2

分子式C8H10O

分子量122.16

展开


  • Mass

    MS-NW-6674          
    o-methylbenzyl alcohol
    C8H10O              (Mass of molecular ion:    122)
    

       Source Temperature: 240 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       4.6
          28.0       2.4
          29.0       2.4
          31.0       2.2
          37.0       1.1
          38.0       2.5
          39.0      13.4
          40.0       1.4
          41.0       3.5
          43.0       1.4
          50.0       5.2
          51.0      13.3
          52.0       4.4
          53.0       3.1
          60.0       4.4
          60.5       1.0
          61.0       1.4
          62.0       3.0
          63.0       7.1
          64.0       1.9
          65.0      13.8
          66.0       1.4
          74.0       1.5
          75.0       1.2
          76.0       1.0
          77.0      32.7
          78.0      14.1
          79.0      35.1
          80.0       2.6
          89.0       3.6
          90.0       1.3
          91.0      33.1
          92.0       3.7
          93.0      19.7
          94.0       1.8
         102.0       1.5
         103.0      12.8
         104.0     100.0
         105.0      16.5
         106.0       2.1
         107.0      33.2
         108.0       2.8
         119.0       3.5
         120.0       1.4
         121.0       5.8
         122.0      31.6
         123.0       2.9
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H10 O 0.041 g : 0.5 ml CDCl3
    o-methylbenzyl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.47 to 7.00 B 4.633 C 2.322 D 1.90

         Hz     ppm     Int.
    

        658.63   7.355     33
        656.81   7.334     25
        655.00   7.314     59
        653.69   7.299     54
        651.13   7.271     82
        649.38   7.251     68
        648.69   7.244     78
        646.63   7.221     68
        643.63   7.187    382
        640.38   7.151    327
        637.69   7.121     45
        415.06   4.635    641
        208.13   2.324   1000
        170.19   1.901    700
    


  • 1H NMR 399.65 MHz
    C8 H10 O 0.042 g : 0.5 ml CDCl3
    o-methylbenzyl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 7.304 B *2 7.18 C *2 7.17 D *1 7.14 E 4.606 F 2.306 G 2.15 J(E,G)=5.3HZ. B,C AND D WERE CONFIRMED BY LAOCN PROGRAM.

         Hz     ppm     Int.
    

       2923.71   7.316     79
       2922.12   7.312     60
       2921.63   7.311     58
       2921.14   7.310     53
       2920.29   7.308     52
       2919.56   7.306     48
       2918.09   7.302    104
       2914.79   7.294    104
       2878.91   7.204     31
       2874.02   7.192    131
       2872.07   7.187    141
       2868.53   7.178    389
       2865.23   7.170    261
       2863.04   7.164    175
       2859.01   7.154    165
       2855.71   7.146     97
       2853.64   7.141     40
       2853.15   7.140     38
       2852.66   7.138     40
       2849.98   7.132     51
       1843.75   4.614    227
       1838.50   4.601    228
        921.88   2.307   1000
        866.21   2.168     55
        860.84   2.154    133
        855.22   2.140     50
    

in CDCl3



KBr disc



liquid film



nujol mull



4880 A,200 M,powder