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MS-IW-0054 2-chloroethyl p-toluenesulfonate C9H11ClO3S (Mass of molecular ion: 234)
Source Temperature: 260 °C Sample Temperature: 160 °C Reservoir, 75 eV
27.0 3.5 28.0 1.3 39.0 5.1 41.0 1.5 50.0 1.3 51.0 2.4 62.0 1.3 63.0 6.9 64.0 1.3 65.0 17.0 66.0 1.0 77.0 2.0 79.0 1.3 89.0 4.6 90.0 2.8 91.0 83.4 92.0 8.4 107.0 3.1 108.0 2.0 139.0 1.1 155.0 100.0 156.0 8.6 157.0 5.1 172.0 13.2 173.0 1.1 185.0 6.5 234.0 15.2 235.0 1.7 236.0 5.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H11 Cl O3 S 0.05 ml : 0.5 ml CDCl3 2-chloroethyl p-toluenesulfonate Assign. Shift(ppm)
A 7.799 B 7.369 C 4.234 D 3.656 E 2.448
Hz ppm Int.
3123.17 7.815 86 3121.22 7.810 411 3119.26 7.805 149 3114.62 7.794 167 3112.67 7.789 438 3110.96 7.785 82 2948.73 7.379 342 2940.80 7.359 306 2940.19 7.357 289 1697.88 4.249 385 1692.14 4.235 578 1686.28 4.220 408 1466.67 3.670 418 1460.82 3.656 596 1455.08 3.641 377 978.39 2.449 1000
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