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MS-NW-6446 m-methoxybenzyl alcohol C8H10O2 (Mass of molecular ion: 138)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.9 18.0 1.2 27.0 3.1 28.0 2.0 29.0 3.4 31.0 3.6 37.0 1.1 38.0 3.4 39.0 11.5 40.0 2.0 41.0 8.6 50.0 5.1 51.0 9.4 52.0 3.1 53.0 2.4 55.0 3.2 61.0 1.0 62.0 2.3 63.0 7.0 64.0 5.3 65.0 10.7 66.0 6.0 67.0 11.1 68.0 1.0 74.0 1.7 75.0 1.1 76.0 1.9 77.0 30.8 78.0 9.7 79.0 13.0 80.0 1.1 89.0 4.0 90.0 1.8 91.0 8.8 92.0 4.9 93.0 1.5 94.0 15.6 95.0 11.0 105.0 18.0 106.0 4.4 107.0 21.1 108.0 2.9 109.0 52.5 110.0 4.5 120.0 1.5 121.0 12.1 122.0 2.8 123.0 6.8 135.0 3.1 136.0 2.2 137.0 23.9 138.0 100.0 139.0 8.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H10 O2 0.05 ml : 0.5 ml CDCl3 m-methoxybenzyl alcohol Assign. Shift(ppm)
A 7.191 B 6.85 C 6.83 D 6.763 E 4.503 F 3.705 G 3.53
Hz ppm Int.
2882.45 7.213 123 2880.62 7.208 31 2876.22 7.197 40 2874.39 7.193 201 2873.29 7.190 93 2867.07 7.174 84 2866.21 7.172 105 2738.40 6.852 124 2737.79 6.851 137 2736.82 6.849 118 2733.15 6.839 113 2731.32 6.835 237 2730.35 6.832 230 2729.61 6.831 272 2729.00 6.829 201 2707.28 6.775 90 2706.79 6.773 91 2706.30 6.772 93 2704.59 6.768 78 2704.22 6.767 77 2703.74 6.766 77 2699.10 6.754 87 2697.27 6.750 96 2695.43 6.745 74 1802.25 4.510 183 1797.49 4.498 181 1480.96 3.706 1000 1414.79 3.541 43 1409.55 3.527 91 1407.96 3.523 68 1404.54 3.515 41
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