图谱信息 供应商 相关产品
网站主页CAS数据库列表 6959-47-3更多图谱2-氯甲基吡啶盐酸盐(6959-47-3)Raman光谱

2-氯甲基吡啶盐酸盐

产品名称 2-氯甲基吡啶盐酸盐

CAS号6959-47-3

分子式C6H7Cl2N

分子量164.03

展开


  • Mass

    MS-NW-8693          
    2-(chloromethyl)pyridine hydrochloride
    C6H6ClN HCl         (Mass of molecular ion:    127)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          17.0       5.7
          18.0      26.5
          26.0       2.0
          27.0       2.1
          28.0       1.6
          35.0       1.8
          36.0      13.2
          37.0       2.5
          38.0       6.8
          39.0      12.1
          40.0       1.4
          41.0       1.8
          45.5       1.1
          49.0       1.7
          50.0       5.1
          51.0      11.2
          52.0       6.0
          53.0       2.7
          61.0       1.4
          62.0       2.4
          63.0       6.5
          64.0       8.3
          65.0      35.1
          66.0       4.0
          73.0       1.4
          75.0       1.0
          78.0      20.0
          79.0       4.0
          80.0       4.3
          90.0       1.0
          91.0       6.9
          92.0      58.2
          93.0       6.8
          99.0       1.4
         100.0       1.6
         108.0       8.4
         109.0       4.3
         126.0       1.0
         127.0     100.0
         128.0       7.6
         129.0      32.7
         130.0       2.3
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H6 Cl N 0.050 g : 0.5 ml CDCl3
    2-(chloromethyl)pyridine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.821 B 8.525 C 8.152 D 7.994 E 5.245

         Hz     ppm     Int.
    

        794.38   8.870     83
        793.63   8.862     97
        792.69   8.851    112
        792.06   8.844    106
        788.69   8.807     98
        788.00   8.799    110
        787.00   8.788    127
        786.25   8.780    116
        773.50   8.637     57
        771.94   8.620     55
        765.50   8.548    124
        764.00   8.531    119
        757.88   8.463    116
        756.13   8.443    107
        733.13   8.186    162
        725.63   8.103    102
        725.00   8.096    100
        722.31   8.066     95
        720.94   8.050     79
        716.63   8.002     79
        715.00   7.984    104
        713.31   7.965     65
        708.88   7.916     55
        707.75   7.903     52
        469.75   5.246   1000
    

in CDCl3



KBr disc



liquid film



nujol mull