2-甲氧基苯甲醇

Mass

MS-NW-6430          
o-methoxybenzyl alcohol
C8H10O2             (Mass of molecular ion:    138)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       2.6
      18.0       2.0
      27.0       4.1
      28.0       3.5
      29.0       4.0
      31.0       3.5
      33.0       1.6
      37.0       1.5
      38.0       3.8
      39.0      13.9
      40.0       2.3
      41.0       6.0
      43.0       1.0
      50.0       6.9
      51.0      16.5
      52.0       4.9
      53.0       2.8
      55.0       3.3
      61.0       1.2
      61.5       1.1
      62.0       2.3
      63.0       6.3
      64.0       3.3
      65.0      12.6
      66.0       3.7
      67.0       3.9
      74.0       1.9
      75.0       1.5
      76.0       4.5
      77.0      46.7
      78.0      15.2
      79.0      15.9
      80.0       1.2
      89.0       2.7
      90.0       3.1
      91.0      34.3
      92.0       6.8
      93.0       3.1
      94.0      11.9
      95.0      11.1
     104.0       2.1
     105.0      51.5
     106.0      21.3
     107.0      37.5
     108.0       4.1
     109.0      33.3
     110.0       3.4
     119.0       5.4
     120.0       6.3
     121.0      18.8
     122.0       6.5
     123.0      18.8
     124.0       1.5
     135.0       2.9
     136.0       1.7
     137.0      29.1
     138.0     100.0
     139.0       8.6

Assign. Shift(ppm) A 7.25 B 7.23 C 6.896 D 6.806 E 4.615 F 3.752 G 3.07 J(E,G)=3.7HZ

     Hz     ppm     Int.

   2900.88   7.259     67
   2900.51   7.258     75
   2899.78   7.256     73
   2899.17   7.255     93
   2898.68   7.254     93
   2893.55   7.241    124
   2893.19   7.240    116
   2892.46   7.238    102
   2891.85   7.236    144
   2891.36   7.235    133
   2886.11   7.222     99
   2885.62   7.221    103
   2884.28   7.218     73
   2883.79   7.216     80
   2878.05   7.202     79
   2876.59   7.198     86
   2876.22   7.197     74
   2763.79   6.916     78
   2762.82   6.914     86
   2756.35   6.897    129
   2755.37   6.895    144
   2749.02   6.879     68
   2747.92   6.876     74
   2724.49   6.818    118
   2723.75   6.816    118
   2716.31   6.797    112
   2715.58   6.795    111
   1846.19   4.620    127
   1842.53   4.611    138
   1499.76   3.753   1000
   1228.03   3.073     60