图谱信息 供应商 相关产品
网站主页 > CAS数据库列表  > 5111-70-6更多图谱  >5-甲氧基-1-茚酮(5111-70-6)质谱(MS)

5-甲氧基-1-茚酮

CAS号5111-70-6

分子式C10H10O2

分子量162.19

展开


  • Mass

    MS-NW-8701          
    5-methoxy-1-indanone
    C10H10O2            (Mass of molecular ion:    162)
    

       Source Temperature: 270 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          27.0       1.3
          38.0       1.3
          39.0       4.4
          41.0       1.1
          50.0       3.0
          51.0       5.5
          52.0       1.4
          53.0       1.1
          62.0       3.2
          63.0      10.9
          64.0       2.7
          65.0       7.5
          74.0       2.4
          75.0       2.7
          76.0       2.2
          77.0       6.5
          78.0       3.4
          79.0       1.8
          81.0       1.0
          89.0       6.1
          90.0       4.4
          91.0      15.5
          92.0       2.4
         102.0       2.4
         103.0       5.6
         104.0       7.0
         105.0       3.2
         106.0       9.8
         107.0       1.1
         118.0       3.9
         119.0      11.7
         120.0       1.1
         131.0       1.9
         132.0       1.4
         133.0       9.0
         134.0      28.9
         135.0       4.0
         147.0       3.3
         161.0      55.5
         162.0     100.0
         163.0      10.9
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C10 H10 O2 0.052 g : 0.5 ml DMSO-d6
    5-methoxy-1-indanone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.560 B 7.078 C 6.955 D 3.863 E 3.040 F 2.58

         Hz     ppm     Int.
    

       3025.88   7.572    131
       3017.46   7.551    140
       2829.83   7.081    102
       2827.88   7.076    107
       2784.91   6.969     78
       2782.59   6.963     70
       2776.37   6.948     73
       2774.05   6.942     66
       1543.82   3.863   1000
       1221.07   3.056     82
       1215.33   3.041     96
       1209.35   3.027     94
       1036.13   2.593    164
       1033.69   2.587     55
       1032.23   2.583     85
       1030.15   2.578    134
       1028.32   2.574     86
       1026.86   2.570     52
       1024.29   2.563    137
    

in DMSO-d6



KBr disc



nujol mull