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MS-NW-3360 indoline C8H9N (Mass of molecular ion: 119)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 1.1 28.0 1.5 38.0 1.7 39.0 5.1 41.0 1.0 43.0 2.6 50.0 1.9 51.0 3.2 52.0 1.7 58.0 1.3 58.5 7.8 59.0 3.5 59.5 2.3 62.0 2.0 63.0 5.7 64.0 2.4 65.0 6.6 77.0 1.2 89.0 8.2 90.0 7.8 91.0 21.9 92.0 2.3 116.0 1.8 117.0 22.2 118.0 100.0 119.0 63.8 120.0 5.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 N 0.04 ml : 0.5 ml CDCl3 indoline Assign. Shift(ppm)
A 7.08 B 6.98 C 6.69 D 6.61 E 3.64 F 3.49 G 3.00
Hz ppm Int.
641.94 7.168 32 640.69 7.154 80 639.69 7.143 192 638.63 7.131 252 638.25 7.127 270 637.56 7.119 245 636.50 7.107 121 635.56 7.097 98 634.81 7.089 155 634.00 7.080 178 632.75 7.066 285 632.06 7.058 356 631.19 7.048 431 630.50 7.040 372 629.44 7.029 178 627.94 7.012 243 627.25 7.004 437 626.50 6.996 355 625.88 6.989 277 622.69 6.953 32 622.25 6.948 34 621.56 6.941 31 620.44 6.928 184 619.81 6.921 353 619.06 6.913 306 618.25 6.904 272 617.56 6.896 153 605.13 6.757 352 603.81 6.742 545 601.56 6.717 30 596.88 6.665 523 594.56 6.639 567 590.50 6.594 214 589.25 6.580 198 587.06 6.555 337 586.63 6.551 324 335.31 3.744 32 325.75 3.638 134 325.19 3.631 135 324.81 3.627 135 323.94 3.618 130 322.44 3.601 524 320.75 3.582 527 316.63 3.536 64 314.69 3.514 544 313.44 3.500 678 312.75 3.493 1000 312.38 3.488 941 305.63 3.413 893 304.56 3.401 916 274.69 3.068 485 270.88 3.025 35 270.56 3.021 36 267.25 2.985 537 266.81 2.980 540 258.81 2.890 193 258.38 2.885 192
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