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MS-NW-3089 1,2-dihydronaphthalene C10H10 (Mass of molecular ion: 130)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 1.4 39.0 3.8 50.0 3.6 51.0 9.1 52.0 1.6 62.0 1.7 63.0 5.9 63.5 1.0 64.0 8.3 65.0 3.6 74.0 2.4 75.0 2.7 76.0 2.1 77.0 5.3 78.0 2.2 89.0 2.0 91.0 1.3 101.0 1.6 102.0 4.5 103.0 1.5 104.0 1.4 115.0 38.2 116.0 3.7 126.0 2.9 127.0 15.0 128.0 35.0 129.0 71.3 130.0 100.0 131.0 10.9 132.0 1.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H10 0.05 ml : 0.5 ml CDCl3 1,2-dihydronaphthalene Assign. Shift(ppm)
A 7.29 to 6.85 B 6.421 C 5.988 D 2.75 E 2.28 J(B,C)=9.6HZ. J(B,E)=1.7HZ. J(C,E)=4.2HZ.
Hz ppm Int.
642.50 7.174 33 641.81 7.167 47 638.38 7.128 108 635.44 7.096 278 632.81 7.066 1000 629.94 7.034 304 628.31 7.016 198 624.13 6.969 134 621.50 6.940 41 620.38 6.927 61 618.44 6.906 40 582.75 6.507 71 581.00 6.488 134 579.25 6.468 72 573.13 6.400 106 571.44 6.381 216 569.69 6.361 120 544.06 6.075 110 539.81 6.028 216 535.63 5.981 102 534.50 5.969 74 530.19 5.920 131 526.00 5.874 63 256.63 2.866 83 255.00 2.848 94 247.75 2.767 228 239.69 2.677 251 237.19 2.649 35 213.81 2.388 81 213.00 2.379 97 212.31 2.371 97 211.31 2.360 88 209.81 2.343 92 208.88 2.333 102 208.13 2.324 103 207.13 2.313 122 205.38 2.294 106 204.13 2.280 140 202.56 2.262 122 201.38 2.249 111 199.88 2.232 115 198.38 2.216 99 196.63 2.196 76 194.81 2.176 45 194.19 2.169 44 194.06 2.167 44 192.38 2.149 70 190.69 2.130 39
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