-
MS-NW-4687 n-propyl-sec-butylamine C7H17N (Mass of molecular ion: 115)
Source Temperature: 260 °C Sample Temperature: 170 °C Reservoir, 75 eV
15.0 1.3 18.0 1.6 27.0 7.7 28.0 5.2 29.0 8.5 30.0 39.0 39.0 3.8 41.0 13.5 42.0 5.5 43.0 10.5 44.0 48.5 45.0 1.4 55.0 2.6 56.0 5.1 57.0 6.8 58.0 15.8 70.0 2.2 72.0 2.4 84.0 2.0 86.0 100.0 87.0 5.9 100.0 12.7 114.0 1.7 115.0 1.1
90 MHz in CDCl3
-
1H NMR 89.56 MHz C7 H17 N 0.04 ml : 0.5 ml CDCl3 N-propyl-sec-butylamine Assign. Shift(ppm)
A 2.56 B 2.73 to 2.34 C 1.78 to 1.17 D 1.17 E 0.990 F 1.02 to 0.77
Hz ppm Int.
237.25 2.650 128 235.31 2.628 107 230.31 2.572 182 228.63 2.553 254 225.50 2.518 83 225.19 2.515 76 224.81 2.511 77 224.13 2.503 75 222.44 2.484 142 221.44 2.473 156 144.69 1.616 89 138.75 1.550 89 137.63 1.537 113 137.00 1.530 116 135.81 1.517 88 130.81 1.461 106 129.94 1.451 170 128.75 1.438 132 127.88 1.428 94 122.81 1.372 165 121.69 1.359 177 120.94 1.351 78 115.31 1.288 92 114.69 1.281 104 108.38 1.211 87 105.50 1.178 68 105.13 1.174 72 104.25 1.165 71 103.75 1.159 70 94.88 1.060 909 92.81 1.037 66 90.06 1.006 148 88.63 0.990 1000 87.13 0.973 224 86.25 0.964 317 85.38 0.954 248 82.50 0.922 446 79.31 0.886 359 78.75 0.880 433 75.81 0.847 103 74.75 0.835 170 73.50 0.821 121 72.69 0.812 101 71.56 0.800 149 70.13 0.784 95
更多供应商