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网站主页CAS数据库列表 349-88-2更多图谱4-氟苯磺酰氯(349-88-2)Raman光谱

4-氟苯磺酰氯

产品名称 4-氟苯磺酰氯

CAS号349-88-2

分子式C6H4ClFO2S

分子量194.61

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  • Mass

    MS-NW-6621          
    p-fluorobenzenesulfonyl chloride
    C6H4ClFO2S          (Mass of molecular ion:    194)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       3.2
          28.0      10.5
          31.0       1.3
          32.0       1.9
          36.0       1.8
          37.0       1.2
          38.0       1.1
          39.0       1.3
          45.0       1.1
          48.0       2.3
          50.0       7.0
          51.0       3.9
          57.0       3.6
          61.0       1.1
          62.0       1.4
          63.0       1.7
          64.0       3.6
          65.0       1.0
          68.0       3.0
          69.0       6.3
          74.0       4.5
          75.0      24.3
          76.0       2.3
          83.0       4.6
          84.0       1.0
          93.0       1.3
          94.0       3.4
          95.0     100.0
          96.0       8.6
         108.0       1.0
         111.0       1.4
         115.0       1.3
         127.0       2.3
         128.0       2.7
         130.0       1.3
         143.0       3.0
         159.0      67.4
         160.0       5.4
         161.0       3.5
         194.0      11.2
         196.0       4.3
         222.0       1.0
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H4 Cl F O2 S 0.046 g : 0.5 ml CDCl3
    p-fluorobenzenesulfonyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.082 B 7.303 J(A,B)=9.2 Hz. J(A,F-19)=4.8 Hz. J(B, F-19)=8.0 Hz.

         Hz     ppm     Int.
    

        734.50   8.202     78
        731.50   8.168    728
        729.31   8.144    271
        726.69   8.115    769
        724.50   8.090    481
        723.56   8.080     89
        722.31   8.066   1000
        719.75   8.037    304
        717.50   8.012    969
        714.50   7.978    132
        665.56   7.432    113
        662.56   7.398    961
        660.31   7.373    283
        659.19   7.361     51
        657.56   7.343    124
        655.56   7.320    260
        654.56   7.309    975
        653.38   7.296    826
        652.31   7.284    333
        651.25   7.272     83
        650.44   7.263    431
        647.56   7.231    246
        645.38   7.207    779
        643.81   7.189     55
        643.13   7.181     51
        642.38   7.173     97
    

in CDCl3



KBr disc



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