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MS-NW-8884 1,2-dichloro-3-nitrobenzene C6H3Cl2NO2 (Mass of molecular ion: 191)
Source Temperature: 280 °C Sample Temperature: 140 °C Reservoir, 75 eV
28.0 3.5 30.0 40.2 36.0 3.2 37.0 3.9 38.0 3.2 39.0 1.9 46.0 1.0 49.0 4.3 50.0 8.5 51.0 2.8 61.0 4.4 62.0 3.1 63.0 6.7 72.0 2.8 73.0 12.5 74.0 42.4 75.0 39.2 76.0 2.7 83.0 2.3 84.0 17.7 85.0 11.4 86.0 6.5 87.0 4.2 88.0 1.0 97.0 2.4 98.0 1.9 107.0 3.2 108.0 2.8 109.0 94.5 110.0 18.5 111.0 31.0 112.0 5.8 119.0 2.4 121.0 1.7 126.0 2.5 128.0 1.1 133.0 67.6 134.0 3.9 135.0 43.7 136.0 2.5 137.0 7.1 144.0 1.4 145.0 100.0 146.0 7.5 147.0 63.6 148.0 4.4 149.0 10.3 161.0 22.8 162.0 1.6 163.0 14.7 164.0 1.0 165.0 2.5 175.0 2.1 177.0 1.4 191.0 96.7 192.0 6.9 193.0 62.4 194.0 4.4 195.0 10.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H3 Cl2 N O2 0.05 ml : 0.5 ml CDCl3 1,2-dichloro-3-nitrobenzene Assign. Shift(ppm)
A 7.70 B 7.69 C 7.37 A AND B WERE CONFIRMED BY LAOCN PROGRAM.
Hz ppm Int.
695.38 7.765 254 694.63 7.757 447 693.63 7.745 402 692.81 7.736 334 686.50 7.666 926 685.75 7.657 1000 667.63 7.455 575 660.56 7.376 315 658.69 7.355 227 651.63 7.276 274