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MS-IW-9271 1,3-dichloro-2-fluorobenzene C6H3Cl2F (Mass of molecular ion: 164)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
31.0 1.5 37.0 1.7 49.0 1.0 50.0 3.1 61.0 2.1 62.0 1.7 63.0 1.9 64.0 4.6 65.0 1.4 68.0 5.0 69.0 1.4 73.0 2.1 74.0 5.2 75.0 1.7 82.0 6.2 83.0 4.1 84.0 2.2 92.0 2.4 93.0 9.0 94.0 5.3 103.0 1.1 104.0 1.1 109.0 6.6 111.0 2.1 128.0 4.8 129.0 34.7 130.0 3.9 131.0 11.2 164.0 100.0 165.0 6.9 166.0 63.7 167.0 4.3 168.0 10.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H3 Cl2 F 0.040 g : 0.5 ml CDCl3 1,3-dichloro-2-fluorobenzene Assign. Shift(ppm)
A 7.303 B 7.028
Hz ppm Int.
2926.51 7.323 808 2919.92 7.307 846 2918.33 7.303 1000 2911.87 7.287 952 2905.15 7.270 25 2817.26 7.050 318 2815.67 7.046 313 2809.45 7.030 388 2808.84 7.029 347 2807.74 7.026 400 2801.03 7.009 244 2799.44 7.005 236
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