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网站主页CAS数据库列表 2039-76-1更多图谱3-乙酰基菲(2039-76-1)Raman光谱

3-乙酰基菲

产品名称 3-乙酰基菲

CAS号2039-76-1

分子式C16H12O

分子量220.27

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  • Mass

    MS-NW-6198          
    3-acetylphenanthrene
    C16H12O             (Mass of molecular ion:    220)
    

       Source Temperature: 150 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       2.8
          43.0       4.4
          51.0       1.1
          62.0       1.0
          63.0       1.5
          74.0       1.9
          75.0       4.3
          76.0       1.0
          82.5       1.1
          87.0       2.4
          87.5       1.5
          88.0      19.0
          88.5       7.8
          89.0       1.5
          94.5       1.9
          95.0       1.0
          96.0       2.7
          98.0       1.2
          99.0       1.1
         102.5       5.7
         103.0       1.1
         110.0       1.5
         126.0       1.1
         149.0       1.2
         150.0       5.8
         151.0      11.7
         152.0       2.1
         174.0       2.8
         175.0       4.3
         176.0      29.1
         177.0      50.4
         178.0       8.4
         189.0       2.7
         190.0       1.0
         191.0       1.5
         205.0     100.0
         206.0      17.0
         207.0       1.6
         220.0      80.9
         221.0      14.3
         222.0       1.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C16 H12 O 0.041 g : 0.5 ml CDCl3
    3-acetylphenanthrene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.230 B 8.704 C 8.071 D 7.86 E 7.855 F 7.782 G 7.680 J 7.68 K 7.609 L 2.739 ASSIGNEG BY H-H COSY.

         Hz     ppm     Int.
    

       3689.45   9.232    113
       3688.48   9.230    116
       3483.64   8.717     69
       3483.15   8.716     71
       3475.46   8.697     71
       3474.85   8.695     73
       3230.96   8.085     84
       3229.25   8.081     87
       3222.66   8.064    103
       3220.95   8.060    105
       3147.09   7.875     66
       3146.36   7.873     67
       3142.94   7.865    139
       3140.01   7.857     85
       3138.55   7.854     84
       3134.64   7.844    114
       3115.48   7.796     82
       3106.69   7.774    123
       3073.12   7.690    154
       3067.50   7.676     67
       3066.16   7.673     87
       3064.82   7.669    115
       3059.33   7.656     62
       3057.86   7.652     58
       3047.85   7.627     68
       3046.51   7.623     74
       3040.77   7.609     52
       3039.92   7.607     77
       3038.82   7.604     72
       3032.96   7.590     38
       3031.74   7.586     36
       1094.73   2.740   1000
    

in CDCl3



KBr disc



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