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MS-IW-7460 alpha-bromo-p-tolunitrile C8H6BrN (Mass of molecular ion: 195)
Source Temperature: 150 °C Sample Temperature: 100 °C Direct, 75 eV
38.0 1.2 39.0 3.1 50.0 2.0 51.0 1.8 57.5 1.8 58.0 1.6 61.0 1.0 62.0 2.5 63.0 4.7 64.0 1.9 88.0 2.3 89.0 14.2 90.0 3.2 114.0 1.3 115.0 1.6 116.0 100.0 117.0 9.4 195.0 7.0 197.0 6.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H6 Br N 0.033 g : 0.5 ml CDCl3 alpha-bromo-p-tolunitrile Assign. Shift(ppm)
A 7.63 B 7.50 C 4.478
Hz ppm Int.
689.63 7.701 174 688.81 7.692 125 687.50 7.677 89 686.31 7.664 38 685.56 7.655 43 683.31 7.630 155 681.06 7.605 610 674.75 7.535 560 672.50 7.509 135 670.63 7.489 46 670.31 7.485 47 668.31 7.463 86 666.19 7.439 151 401.13 4.479 1000 397.25 4.436 31 396.88 4.432 28
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