-
MS-NW-6360 2,6-dichlorobenzyl alcohol C7H6Cl2O (Mass of molecular ion: 176)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 1.4 26.0 1.1 27.0 2.2 28.0 4.6 29.0 7.1 30.0 1.1 31.0 7.0 36.0 5.5 37.0 4.1 38.0 6.0 39.0 5.6 43.0 2.8 44.0 2.0 49.0 3.0 50.0 13.9 51.0 19.1 52.0 11.6 52.5 1.1 53.0 1.0 55.0 1.4 56.0 2.1 60.0 1.2 61.0 4.7 61.5 1.3 62.0 6.1 63.0 7.0 65.0 1.2 70.0 2.2 70.5 1.1 72.0 1.3 73.0 6.7 74.0 12.6 75.0 34.4 76.0 7.8 77.0 100.0 78.0 9.3 84.0 4.2 85.0 4.8 86.0 2.9 87.0 2.7 87.5 2.6 88.5 1.5 89.0 5.8 91.0 9.8 92.0 7.9 97.0 1.6 99.0 1.7 105.0 2.4 109.0 5.2 110.0 3.2 111.0 36.9 112.0 7.2 113.0 55.2 114.0 5.0 115.0 14.9 116.0 1.2 123.0 8.4 124.0 2.6 125.0 3.5 126.0 1.1 133.0 1.1 139.0 32.4 140.0 21.2 141.0 81.8 142.0 12.6 143.0 24.1 144.0 2.0 145.0 3.0 146.0 3.3 147.0 5.1 148.0 2.5 149.0 2.4 158.0 1.1 159.0 11.7 160.0 1.9 161.0 7.6 162.0 1.0 163.0 1.3 173.0 3.3 175.0 14.6 176.0 44.8 177.0 11.6 178.0 28.9 179.0 3.9 180.0 4.9
90 MHz in CDCl3
-
1H NMR 89.56 MHz C7 H6 Cl2 O 0.040 g : 0.5 ml CDCl3 2,6-dichlorobenzyl alcohol Assign. Shift(ppm)
A 7.32 B 7.178 C 4.956 D 2.13
Hz ppm Int.
662.25 7.395 150 658.25 7.350 215 652.38 7.285 676 648.00 7.236 514 642.81 7.178 209 638.13 7.126 93 632.94 7.068 65 446.44 4.985 31 443.88 4.957 1000 190.38 2.126 156 188.06 2.100 55
更多供应商