-
MS-IW-0582 2,4-dibromo-1-fluorobenzene C6H3Br2F (Mass of molecular ion: 252)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
31.0 1.5 37.0 2.4 38.0 1.2 47.0 2.4 49.0 1.5 50.0 8.2 61.0 3.0 62.0 2.5 63.0 1.7 68.0 8.1 73.0 2.4 74.0 9.7 75.0 3.6 86.0 2.7 86.5 1.3 87.0 2.8 87.5 1.3 92.0 3.4 93.0 11.6 94.0 45.6 95.0 3.1 126.0 3.5 127.0 6.8 128.0 3.9 153.0 1.0 172.0 1.3 173.0 37.1 174.0 3.7 175.0 36.2 176.0 2.4 252.0 51.2 253.0 3.8 254.0 100.0 255.0 6.8 256.0 48.6 257.0 3.2
400 MHz in CDCl3
-
1H NMR 399.65 MHz C6 H3 Br2 F 0.05 ml : 0.5 ml CDCl3 2,4-dibromo-1-fluorobenzene Assign. Shift(ppm)
A 7.657 B 7.363 C 6.980
Hz ppm Int.
3064.45 7.668 745 3062.01 7.662 800 3058.35 7.653 776 3055.91 7.647 825 2951.17 7.385 410 2948.73 7.379 414 2946.90 7.374 436 2944.46 7.368 419 2942.38 7.363 459 2938.11 7.352 573 2935.67 7.346 474 2797.97 7.002 779 2789.55 6.980 1000 2789.18 6.980 938 2783.20 6.965 27 2781.01 6.959 736
更多供应商