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MS-NW-6399 diethyl aminomalonate hydrochloride C7H13NO4 HCl (Mass of molecular ion: 175)
Source Temperature: 240 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.2 17.0 2.1 18.0 9.8 19.0 2.9 26.0 3.0 27.0 15.5 28.0 50.7 29.0 51.6 30.0 2.5 31.0 6.1 36.0 7.7 38.0 2.5 43.0 2.2 44.0 4.0 45.0 5.5 46.0 10.8 47.0 2.7 56.0 4.8 57.0 5.7 73.0 1.1 74.0 48.7 75.0 2.0 100.0 3.2 101.0 1.6 102.0 100.0 103.0 6.6 129.0 3.4 130.0 1.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H13 N O4 0.041 g : 0.5 ml CDCl3 diethyl aminomalonate hydrochloride Assign. Shift(ppm)
A 9. B 5.040 C 4.337 D 1.326
Hz ppm Int.
823.31 9.193 38 451.44 5.041 128 399.69 4.463 74 392.69 4.385 256 385.81 4.308 315 383.44 4.282 37 378.69 4.229 117 125.88 1.406 399 120.88 1.350 30 118.75 1.326 1000 115.50 1.290 37 111.56 1.246 367 109.94 1.228 45
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