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MassMS-NW-6327 1-amino-9-fluorenone C13H9NO (Mass of molecular ion: 195)
Source Temperature: 240 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 4.3 27.0 1.1 31.0 2.4 39.0 3.0 44.0 1.3 45.0 1.7 50.0 1.3 51.0 1.9 52.0 1.1 62.0 1.7 63.0 2.8 65.0 2.3 66.0 10.5 69.0 1.1 69.5 3.4 70.0 1.9 70.5 3.0 74.0 1.4 75.0 1.6 76.0 1.1 77.0 1.4 82.5 1.8 83.5 6.3 84.0 1.7 87.0 1.5 88.0 1.1 89.0 1.7 91.0 1.5 97.5 3.6 98.0 2.2 113.0 1.7 114.0 1.8 115.0 1.9 132.0 6.8 133.0 5.1 138.0 1.4 139.0 14.0 140.0 6.6 141.0 1.1 164.0 1.6 166.0 5.0 167.0 4.8 168.0 12.8 169.0 1.9 194.0 1.3 195.0 100.0 196.0 15.0 197.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H9 N O 0.035 g : 0.5 ml CDCl3 1-amino-9-fluorenone 
Assign. Shift(ppm)
A 7.596 B 7.451 C 7.407 D 7.251 E 7.180 F 6.802 G 6.472 J 5.53
Hz ppm Int.3039.79 7.607 715 3036.25 7.598 85 3032.35 7.588 793 2983.03 7.465 468 2975.71 7.446 994 2967.41 7.426 509 2966.31 7.423 520 2963.50 7.416 79 2960.08 7.407 744 2958.98 7.404 744 2955.08 7.395 68 2952.64 7.389 329 2951.54 7.386 327 2905.52 7.271 442 2904.42 7.268 454 2898.19 7.252 780 2897.09 7.250 765 2890.87 7.234 340 2889.77 7.231 345 2886.60 7.223 38 2877.56 7.201 531 2870.36 7.183 686 2869.26 7.180 694 2865.60 7.171 65 2862.06 7.162 620 2858.15 7.152 32 2721.68 6.811 1000 2718.75 6.803 92 2714.60 6.793 917 2590.58 6.483 948 2586.91 6.473 67 2582.15 6.462 899 2209.47 5.529 492
in CDCl3
KBr disc
nujol mull
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