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MS-NW-7151 p-nitrobenzenesulfonamide C6H6N2O4S (Mass of molecular ion: 202)
Source Temperature: 220 °C Sample Temperature: 110 °C Direct, 75 eV
16.0 1.1 18.0 2.5 27.0 1.7 28.0 3.3 30.0 17.0 32.0 1.0 37.0 2.8 38.0 7.1 39.0 12.7 41.0 1.2 45.0 2.5 46.0 2.7 48.0 3.7 49.0 1.5 50.0 60.7 51.0 11.7 52.0 4.4 53.0 4.0 54.0 1.2 58.0 1.0 61.0 2.1 62.0 5.1 63.0 17.0 64.0 30.7 65.0 20.7 66.0 3.7 69.0 3.7 70.0 2.5 73.0 3.3 74.0 23.7 75.0 100.0 76.0 53.1 77.0 6.7 79.0 1.8 80.0 5.8 81.0 4.6 82.0 1.6 90.0 3.3 91.0 3.0 92.0 33.4 93.0 4.9 95.0 1.9 96.0 1.6 106.0 1.6 107.0 2.1 108.0 15.1 109.0 13.1 110.0 1.4 121.0 3.8 122.0 54.3 123.0 5.2 124.0 1.3 138.0 62.0 139.0 40.1 140.0 3.8 156.0 15.9 157.0 1.4 186.0 35.3 187.0 3.2 188.0 2.0 202.0 87.3 203.0 7.4 204.0 5.2 308.0 2.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H6 N2 O4 S 0.041 g : 0.5 ml DMSO-d6 p-nitrobenzenesulfonamide Assign. Shift(ppm)
A 8.434 B 8.098 C 7.77
Hz ppm Int.
3375.40 8.446 865 3373.41 8.441 325 3368.53 8.429 314 3366.39 8.424 1000 3363.95 8.418 152 3242.95 8.115 143 3240.51 8.109 994 3238.53 8.104 342 3233.64 8.092 297 3231.66 8.087 883 3105.16 7.770 875
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