2-Chlorobenzoyl chloride

Mass

MS-NW-0866          
o-chlorobenzoyl chloride
C7H4Cl2O            (Mass of molecular ion:    174)

   Source Temperature: 280 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      28.0       2.4
      36.0       1.8
      37.0       3.6
      37.5       3.2
      38.0       6.7
      39.0       1.0
      49.0       2.7
      50.0      15.6
      51.0       5.0
      55.5       3.4
      56.5       1.0
      61.0       1.9
      69.5       3.2
      70.0       4.4
      70.5       1.5
      71.0       1.0
      73.0       3.2
      74.0       9.3
      75.0      26.7
      76.0       5.7
      84.0       2.1
      85.0       3.7
      87.0       1.3
     110.0       1.0
     111.0      39.3
     112.0       3.0
     113.0      12.9
     139.0     100.0
     140.0       7.8
     141.0      33.2
     142.0       2.5
     174.0       4.0
     176.0       2.5

Assign. Shift(ppm) A 8.07 B 7.68 to 7.25

     Hz     ppm     Int.

    728.75   8.138    171
    727.38   8.122    171
    727.00   8.118    197
    724.94   8.095    148
    721.81   8.060    152
    720.81   8.049    207
    720.44   8.045    183
    718.69   8.025    207
    716.94   8.006     61
    685.00   7.649     41
    677.94   7.570     34
    675.44   7.542    185
    674.50   7.532    107
    674.00   7.526    198
    673.19   7.517    237
    671.69   7.500    562
    671.06   7.493    619
    669.81   7.479   1000
    667.50   7.454    273
    666.31   7.440     76
    665.44   7.431    109
    664.69   7.422     37
    662.88   7.402    261
    660.13   7.371     60
    659.38   7.363    105
    657.38   7.341     99
    653.88   7.302     71
    650.31   7.262     31