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MS-NW-3441 o-allylphenol C9H10O (Mass of molecular ion: 134)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.6 26.0 5.6 27.0 24.7 28.0 1.1 29.0 3.6 37.0 4.6 38.0 11.7 39.0 48.4 40.0 4.4 41.0 4.9 43.0 3.1 49.0 2.5 50.0 18.6 51.0 37.8 52.0 15.0 53.0 14.2 54.0 1.1 55.0 10.3 61.0 4.3 62.0 9.2 63.0 20.5 64.0 5.7 65.0 15.2 66.0 7.6 67.0 1.2 68.0 1.7 73.0 1.5 74.0 7.6 75.0 5.8 76.0 4.1 77.0 62.7 78.0 38.2 79.0 28.3 80.0 2.8 81.0 1.4 85.0 1.0 86.0 1.8 87.0 2.3 88.0 1.2 89.0 12.0 90.0 7.8 91.0 73.7 92.0 8.3 94.0 5.7 102.0 3.0 103.0 12.6 104.0 3.6 105.0 33.9 106.0 6.5 107.0 31.7 108.0 2.9 114.0 1.3 115.0 45.9 116.0 10.5 117.0 13.7 118.0 4.6 119.0 36.3 120.0 3.3 131.0 8.4 132.0 3.3 133.0 38.5 134.0 100.0 135.0 10.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H10 O 10.6 MOL % in CDCl3 o-allylphenol Assign. Shift(ppm)
A 7.12 to 7.05 B 6.89 C 6.78 D 5.971 E 5.4 F 5.11 G 3.380
Hz ppm Int.
638.13 7.126 305 637.50 7.119 355 634.94 7.090 489 634.56 7.086 389 633.06 7.069 409 632.56 7.063 565 632.00 7.057 341 631.44 7.051 379 630.88 7.045 663 630.31 7.038 498 628.56 7.019 819 621.06 6.935 473 619.44 6.917 745 614.31 6.860 339 612.94 6.844 443 609.38 6.805 665 608.31 6.793 421 602.25 6.725 319 601.75 6.719 302 600.25 6.703 275 557.44 6.225 168 551.06 6.153 291 548.00 6.119 162 544.88 6.084 175 541.63 6.048 300 539.88 6.029 209 535.50 5.980 204 533.50 5.957 384 530.38 5.923 313 527.31 5.888 245 524.06 5.852 540 517.94 5.784 355 481.56 5.377 100 466.19 5.206 493 464.63 5.188 971 463.63 5.177 536 463.00 5.170 593 462.19 5.161 1000 460.75 5.145 532 460.25 5.140 332 452.75 5.056 442 452.19 5.050 286 451.31 5.040 318 450.75 5.033 678 449.00 5.014 585 447.00 4.992 431 307.06 3.429 423 305.75 3.414 718 304.31 3.398 422 300.75 3.359 403 299.50 3.345 690 298.13 3.329 397
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