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MS-NW-7390 2,6-difluoropyridine C5H3F2N (Mass of molecular ion: 115)
Source Temperature: 200 °C Sample Temperature: 190 °C Reservoir, 75 eV
26.0 1.0 31.0 5.9 37.0 2.7 38.0 4.2 39.0 5.2 44.0 3.0 49.0 1.7 50.0 4.9 51.0 4.9 52.0 1.5 56.0 1.5 57.0 4.9 57.5 1.2 64.0 6.7 65.0 7.2 68.0 4.4 69.0 7.6 70.0 21.4 71.0 1.6 75.0 3.3 76.0 4.0 88.0 22.3 89.0 2.1 95.0 4.2 96.0 6.5 114.0 1.7 115.0 100.0 116.0 6.0
parameter in CDCl3
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1H NMR 300 MHz C5 H3 F2 N 15 vol% in CDCl3 2,6-difluoropyridine Parameter ppm Hz
D(A) 6.84 D(B) 7.92 D(X) -62.1 J(A,A') 0.55 J(A,B) 7.94 J(A,X) -2.47 J(A,X') 1.19 J(A',B) 7.94 J(A',X) 1.19 J(A',X') 2.47 J(B,X) 7.97 J(B,X') 7.97 J(X,X') -12.23 THOMAS,W.A. & GRIFFIN,G.E. ORG.MAGN.RESON. 2, 503 (1970)
Hz ppm Int.
2392.00 7.973 122 2384.01 7.947 495 2376.05 7.920 716 2368.11 7.894 510 2360.20 7.867 135 2056.16 6.854 870 2055.71 6.852 876 2048.04 6.827 1000
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