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MassMS-NW-5620 3-methyl-2-cyclohexen-1-one C7H10O (Mass of molecular ion: 110)
Source Temperature: 270 °C Sample Temperature: 190 °C Reservoir, 75 eV
26.0 1.0 27.0 7.7 28.0 2.4 29.0 1.1 38.0 2.3 39.0 24.0 40.0 3.3 41.0 6.7 42.0 3.5 50.0 1.8 51.0 2.9 52.0 1.8 53.0 6.8 54.0 26.4 55.0 2.1 65.0 1.3 67.0 5.6 68.0 1.0 77.0 1.2 79.0 1.4 81.0 1.0 82.0 100.0 83.0 5.6 110.0 38.9 111.0 3.2
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C7 H10 O 0.04 ml : 0.5 ml CDCl3 3-methyl-2-cyclohexen-1-one 
Assign. Shift(ppm)
A 5.369 B 2.39 to 2.24 C 2.04 D 1.96
Hz ppm Int.527.81 5.894 120 526.44 5.879 250 525.13 5.864 258 523.75 5.849 131 522.44 5.834 35 218.13 2.436 50 217.13 2.425 75 215.94 2.412 131 213.88 2.389 43 212.44 2.373 112 210.25 2.348 286 208.63 2.330 174 207.75 2.320 179 205.75 2.298 194 203.88 2.277 375 202.25 2.259 228 201.00 2.245 184 200.25 2.236 162 199.88 2.232 159 199.25 2.225 151 198.56 2.218 118 195.94 2.188 35 190.31 2.125 160 188.25 2.102 161 185.63 2.073 123 185.00 2.066 106 183.63 2.051 168 182.50 2.038 200 181.25 2.024 44 179.75 2.008 99 178.69 1.996 90 177.19 1.979 620 176.50 1.971 1000 175.81 1.964 878 175.19 1.957 944 174.38 1.948 499 172.19 1.923 104 171.31 1.913 113 169.50 1.893 56 165.94 1.853 31 163.56 1.827 37
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1H NMR 399.65 MHz C7 H10 O 0.05 ml : 0.5 ml CDCl3 3-methyl-2-cyclohexen-1-one Assign. Shift(ppm)
A 5.857 B 2.328 C 2.31 D 2.00 E 1.97 90MHZ : HSP-03-618
Hz ppm Int.2344.48 5.867 68 2343.14 5.863 197 2341.80 5.860 336 2340.33 5.856 346 2338.99 5.853 213 937.62 2.347 418 935.18 2.340 98 934.45 2.339 102 931.15 2.330 472 929.81 2.327 346 928.34 2.323 230 927.61 2.322 235 926.76 2.319 238 924.07 2.313 522 922.00 2.308 376 921.39 2.306 380 915.77 2.292 236 915.16 2.290 238 810.42 2.028 157 807.98 2.022 63 804.08 2.012 323 799.19 2.000 174 798.10 1.997 330 797.12 1.995 390 790.89 1.979 419 788.33 1.973 935 787.11 1.970 1000
in CDCl3
liquid film
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