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109-04-6

2-Bromopyridine

Product Name 2-Bromopyridine

CAS109-04-6

MFC5H4BrN

MW158

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  • 109-04-6_ms
    Mass 

    MS-NW-2643          
2-bromopyridine
C5H4BrN             (Mass of molecular ion:    157)


       Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV


          26.0       3.2
      27.0       5.7
      28.0       4.2
      37.0       1.3
      38.0       2.3
      39.0       2.8
      49.0       2.1
      50.0      11.3
      51.0      30.9
      52.0       9.1
      75.0       1.5
      76.0       3.3
      77.0       1.1
      78.0     100.0
      78.5       1.1
      79.0       5.9
      79.5       1.1
     157.0      32.4
     158.0       2.0
     159.0      30.8
     160.0       1.9

parameter in CCl4

90 MHz in CDCl3

  • 109-04-6_1hnmr

    1H NMR 300 MHz
    C5 H4 Br N 10 vol% in CCl4
    2-bromopyridine
    ChemicalStructure 
        Parameter     ppm  Hz
    
      D(A)         8.31
      D(B)         7.17
      D(C)         7.46
      D(D)         7.40
       J(A,B)          4.81
       J(A,C)          2.09
       J(A,D)          0.79
       J(B,C)          7.39
       J(B,D)          0.94
       J(C,D)          8.03
     
     SMITH,W.B. & ROARK,J.L. J.PHYS.CHEM. 73, 1049 (1969)
  

         Hz     ppm     Int.


       2496.84   8.323    473
   2496.06   8.320    502
   2494.80   8.316    514
   2494.02   8.313    502
   2492.05   8.307    500
   2491.20   8.304    521
   2490.04   8.300    521
   2489.22   8.297    491
   2247.61   7.492    245
   2245.56   7.485    238
   2240.46   7.468    328
   2239.60   7.465    563
   2238.47   7.462    347
   2237.54   7.458    544
   2232.48   7.442    646
   2230.47   7.435    648
   2224.15   7.414    677
   2223.07   7.410   1000
   2222.11   7.407    756
   2216.14   7.387    335
   2215.25   7.384    423
   2214.11   7.380    263
   2157.39   7.191    478
   2156.17   7.187    465
   2152.59   7.175    478
   2151.32   7.171    498
   2150.30   7.168    462
   2149.08   7.164    412
   2145.52   7.152    395
   2144.26   7.148    383

  • 109-04-6_1hnmr_2

    1H NMR 89.56 MHz
    C5 H4 Br N 0.05 ml : 0.5 ml CDCl3
    2-bromopyridine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             8.36
      B             7.56
      C             7.49
      D             7.26
  

         Hz     ppm     Int.


        752.63   8.404    152
    751.75   8.394    178
    750.75   8.383    193
    749.88   8.373    184
    747.88   8.351    177
    746.38   8.334    235
    745.06   8.320    185
    686.50   7.666    103
    684.50   7.643     95
    680.25   7.596     72
    678.56   7.577    417
    676.56   7.555    421
    673.19   7.517    404
    672.31   7.507   1000
    670.50   7.487    865
    669.75   7.479    656
    666.50   7.442     31
    665.25   7.428    152
    664.25   7.417    141
    662.94   7.403     76
    657.31   7.340     58
    655.88   7.324    440
    653.63   7.299    300
    651.06   7.270    384
    649.63   7.254    257
    648.63   7.243    281
    647.38   7.229    243
    645.06   7.203    216
    642.56   7.175    209

in CDCl3

  • 109-04-6_13cnmr

liquid film

  • 109-04-6_ir1

  • 109-04-6_raman

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