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N,N-Bis(3-aminopropyl)methylamine

Product Name N,N-Bis(3-aminopropyl)methylamine

CAS105-83-9

MFC7H19N3

MW145.25

¹³CNMR

Mass

MS-NW-0990          
3,3'-diamino-n-methyldipropylamine
C7H19N3             (Mass of molecular ion:    145)

   Source Temperature: 250 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      15.0       3.6
      16.0       1.0
      17.0      20.4
      18.0     100.0
      27.0       4.3
      28.0      30.9
      29.0       7.1
      30.0      55.4
      31.0      37.5

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₇ H₁₉ N₃	0.04 ml : 0.5 ml CDCl₃
3,3'-diamino-N-methyldipropylamine

    Assign.     Shift(ppm)

      A             2.725
      B             2.373
      C             2.202
      D             1.608
      E             1.27

     Hz     ppm     Int.

    251.50   2.809    232
    244.56   2.731    565
    237.81   2.656    327
    220.75   2.465    153
    220.38   2.461    153
    213.81   2.388    346
    211.13   2.358     91
    206.25   2.303    270
    197.19   2.202    964
    157.81   1.763     58
    156.75   1.751     65
    152.38   1.702     33
    150.69   1.683    151
    149.81   1.673    197
    146.00   1.631     39
    143.06   1.598    236
    137.88   1.540     53
    135.88   1.518    145
    129.94   1.451     37
    128.81   1.439     38
    113.31   1.266   1000

in CDCl3

liquid film

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