PMK ethyl glycidate NEW

$0.00 25KG

$0.00 5KG

$0.00 1KG

Min. Order1KG
Purity98%~99%
Cas No28578-16-7
Supply Ability20 T each week
Update time2023-08-12

Shandong Huisheng Import & Export Co., Ltd.

2YR

China

Since2020-11-16

AddressRoom 202-9, Building 1, Evergrande Huafu, Dongying Road, Huaiyin District, Jinan City, Shandong Prov

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Chemical Properties

Product Name	PMK ethyl glycidate
CAS No	28578-16-7
EC-No	234-232-0
Min. Order	1KG
Purity	98%~99%
Supply Ability	20 T each week
Release date	2023/08/12

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Product Name:	PMK ethyl glycidate
Synonyms:	3-(1,3-benzodioxol-5-yl)-2-Methyl-;3,4-MDP-2-P intermediate;PMK ethyl glycidate;2-Oxiranecarboxylicacid, 3-(1,3-benzodioxol-5-yl)-2-Methyl-, ethyl ester;ethyl 3-(benzo[d][1,3]dioxol-5-yl)-2-methyloxirane-2-carboxylate;ethyl 3-(1,3-benzodioxol-5-yl)-2-methyloxirane-2-carboxylate;3,4-MDP-2P ethyl ester;cheap 3,4-MDP-2P ethyl ester
CAS:	28578-16-7
MF:	C13H14O5
MW:	250.25
EINECS:	234-232-0
Product Categories:	28578-16-7;1;28578;PMK;Pharm
Mol File:	28578-16-7.mol

PMK ethyl glycidate Chemical Properties

Boiling point	327.8±42.0 °C(Predicted)
density	1.302±0.06 g/cm3(Predicted)
solubility	DMF: 15 mg/ml; DMSO: 30 mg/ml; Ethanol: 10 mg/ml; PBS (pH 7.2): 1 mg/ml
InChI	InChI=1S/C13H14O5/c1-3-15-12(14)13(2)11(18-13)8-4-5-9-10(6-8)17-7-16-9/h4-6,11H,3,7H2,1-2H3
InChIKey	BRILFEZHPXQINW-UHFFFAOYSA-N
SMILES	O1C(C2=CC=C3OCOC3=C2)C1(C)C(OCC)=O

PMK ethyl glycidate Usage And Synthesis

Description	PMK ethyl glycidate is an analytical reference standard categorized as a precursor in the synthesis of methylenedioxy phenethylamines and amphetamines, including 3,4-MDMA. This product is intended for research and forensic applications.
Uses	NSC 195099 can be used as an analytical reference standard.
Application	PMK methyl glycidate is applied as immediate precursors of 3,4-methylenedioxymethamphetamine.
Synthesis	To a solution of piperonal (1, 3.00 g, 19.9 mmol) in CH2Cl2 (100 mL) was added (carbethoxyethylidene)triphenylphosphorane (2,14.5 g, 40.0 mmol), and the reaction mixture was stirred for 24 h at room temperature. The mixture was then concentrated at reduced pressure, and the residue was purified by flash column chromatography on silica gel (hexanes/EtOAc,10:1) to afford olefin 3 (4.45 g, 95%) as a colorless oil: 1H NMR (400 MHz, CDCl3) d 7.58 (s, 1H), 6.92 (d, J = 1.7 Hz, 1H), 6.90 (dd, J = 7.9, 1.7 Hz, 1H), 6.82 (d, J = 8.0 Hz, 1H), 5.97 (s, 2H), 4.24 (q, J = 7.1 Hz, 2H), 2.10 (d, J = 1.6 Hz, 3H),1.33 (t, J = 7.1 Hz, 3H); 13C NMR (100 MHz, CDCl3) d 168.7,147.6, 138.3, 129.9, 126.9, 124.6, 109.5, 108.2, 101.2, 60.7, 14.3,1 4.0; IR (ATR, cm-1): 2981, 2902,1698, 1628, 1502, 1489,1442, 1258, 1224; HRMS (EI) m/z calcd for C13H14O4 (M+) 234.0892, found 234.0895. Fig The synthetic step of PMK ethyl glycidate

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Company Profile Introduction

Shandong Huisheng Import & Export Co., Ltd. is located in Jinan city, Shandong Province, is a collection of domestic trade, international trade in one of the diversified services company. Our goal is to provide customers with high quality solutions and one-stop purchasing experience. At present, the company business scope involves five areas: Organic chemical raw materials, inorganic chemical raw materials, fine chemical raw materials, dangerous chemicals and green environmental protection chemical technology project promotion, and we has also established good relations of cooperation with several well-known enterprises and won the strong support of extensive trust from the new and old customers. Products are widely used in automobile, household appliances, office supplies, mobile phone accessories, routers, food, medical and other fields. At present, our business covers 30 countries, and our customers mainly come from Australia, New Zealand, Canada, Germany, France, Poland, South Korea, Russia, Bangladesh, Vietnam, Kazakhstan, India, Ghana, Nigeria, South Africa, Egypt and other more than 30 countries. The company has a sound quality management system and advanced professional equipment, with a positive attitude to meet the changing needs of customers. We take "quality products, quality service, competitive price, timely delivery" as the purpose, looking forward to greater cooperation with overseas customers on the basis of mutual benefit. Our company provides a wide range of products to meet your various needs. Since its inception, the company has always adhered to the "quality first, customer first, reputation first" business policy, wholeheartedly meet the potential needs of our customers. Under the irresistible situation of economic globalization, our company is willing to cooperate sincerely with enterprises around the world to achieve a win-win situation.