2-Phenylacetamide
Chemical properties:
white flake crystal. Soluble in hot water, ethanol, slightly soluble in cold water, ether and benzene.
Uses:
2-phenylacetamide can be used as an intermediate in organic synthesis and medicine, pesticides and spices. In the pharmaceutical industry, it is the medium of penicillin G and the raw material of the sedative phenobarbital.
Production method:
Put styrene, sulfur, liquid ammonia and water into the autoclave, react at 165℃, about 6.5MPa pressure, and then heat evaporation to drive off hydrogen sulfide gas, add activated carbon decolorization, cooling, crystallization, filtration, drying to obtain phenylacetamide. This method can be improved to pipelined continuous production, styrene and ammonium polysulfide liquid according to the volume ratio of 1:2, through the high pressure pipeline, reaction temperature of 200℃, reaction pressure of 6-7.8MPa, reaction time of 1.5h. The post-treatment process of the reaction products is similar to that of the autoclave batch method. Raw material consumption quota: styrene (99%) 1117kg/t, sulfur (98.5%) 716kg/t, liquid ammonia (99%) 539kg/t, activated carbon 47kg/t.
Another production method is to hydrolyze benzyl chloride (obtained by the reaction of benzyl chloride and sodium cyanide in an aqueous solution of dimethylamine) by heating in sulfuric acid or hydrochloric acid. Add benzonitrile to concentrated hydrochloric acid, stir to dissolve, and react at 50℃ for half an hour. Then slowly add water to precipitate crystallization under cooling, filter after cooling, and wash with ice water to obtain crude products. The crude product is washed with sodium carbonate solution, and then washed with ice water. After drying, more pure phenylacetamide can be obtained. Raw material consumption quota: Benzyl chloride (95%) 1190kg/t, sodium cyanide (95%) 527kg/t, dimethylamine (industrial products) 20kg/t, sodium carbonate (industrial products) 185kg/t, sulfuric acid (92.5%) 1760kg/t.
| Melting Point | 156 °C |
| Boiling Point | 280-290 °C |
Density
| 1.1031 |
| Refractive Index | 1.5589 |
| Storage Condition | Refrigerator |
| pKa | 16.21±0.40 |
Our advantages:
1) Timely communication, reply within 12 hours.You can leave any messages on our whatsapp or send email to us.
2)Selecting raw materials strictly,our products are the highest purity.
3)Reasonable and competitive price.
4) Free sample for your evaluation.Customers only need to undertake the shipping fee for delivery the samples to your destionation.
5)OEM/ODM Available.Trial order is available for testing after samples.
6) Packaging can be customized according to each buyers' special request.
We guarantee that your package will pass 100% through the Mexico US, UK, Australia, Netherlands, Canada, France, Germany, Spain, Belgium, Sweden, Poland, Russian, Ukraine, Kazakhstan, Czech Republic, Slovakia, Portugal.
We have freight forwarders in these countries, and our customs clearance company will clear your parcels without any customs issues, sometimes even 1000 kg. Door to door service. Make sure you receive 100% of the goods. Let you have a good experience of our strong freight capacity.
Company Introduction
hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and development production of reagent tens of thousands of species. our aim is quality strives for the survival. Seek development by credit reputation. Our products have big price advantage in Europe South America and so on .and Our company also has the advantage of high quality in Africa. in the past two years our products has reached more than 30 countries in the world, Europe. South America. North America, southeast Asia, Africa, etc. We welcome all over the world with the best quality and lowest price friend common cooperation and common development!
6.After Sales Service
1) Best quality in your requirement
2)Competitive price in china market
3)Mature technical support
4)Professional logistic support
5 )Full experience of large numberscontainers loading in chinese sea port
6 )Fast shipment by reputed shipping line
7) Packing with pallet as buyer's special request
8) Best service after shipment.
9) Cargoes together with container after-sales service available
10) Full experience in export
11)Raw materials from chinese origin
7. FAQ
What is the way you ship?
Express: FedEx, UPS, EMS, DHL, USPS, TNT, DPD, Aramex etc
Our way of shipping the products is universal and secure.
The company name and other contents related to pharmacy are not written on the package slips.
The way of packing is regularly changed for a secure delivery.
The packages are small in order to avoid unwelcomed questions . If the order is big, then it will be divided into two or more packages
Can the packages be trackable?
YES, we provide tracking number and you can track on internet.
Where do you ship to?
Worldwide.
Do you offer domestic shipping/remail shipping?
Yes we can ship to USA/UK/Canada/Australia/Germany etc warehouse first then to you.
Do you ensure your packing , what about customs, what happens if the package is retained?
We concern a lot about our safety system, we pack the orders as secure as possible. If a package is seized at customs, reships of seized orders will be done provided you have a copy of the letter to show us. If you receive a seizure letter, please contact us immediately with a scanned copy of the seizure letter, and also a new address to have your order reshipped to.
Which payment options are available?
Bitcoin
Western Union
Bank wire
MoneyGram
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