English name: 1-Bromooctadecane
CAS number: 112-89-0
Molecular formula: C18H37Br
Molecular weight: 333.39
EINECS number: 204-013-4
MDL No. : MFCD00000231
Stats
Melting point 25-30 °C(lit.)
Boiling point 214-216 °C12 mm Hg(lit.)
Density 0.976 g/mL at 25 °C(lit.)
Refractive index 1.462-1.464
Flash point >230 °F
Storage conditions Inert atmosphere,Room Temperature
The form is Low Melting Solid
Specific gravity 0.980 (20/4℃)
Color Yellow
Water is insoluble
BRN774145
InChIKeyWSULSMOGMLRGKU-UHFFFAOYSA-N
Safety information
GHS hazard pictograms GHS Hazard pictograms
GHS08
Danger
Hazard Description H304
Precautions P301+P310-P331-P405-P501
Hazard category code 36/37/38
Safety Instructions 22-24/25
WGK Germany3
TSCAYes
Customs Code 29033036
Production method:
It is obtained by the reaction of octadecyl alcohol with hydrogen bromide. The alcohol is heated to 100 ° C, the dry hydrogen bromide is added, and the reaction temperature is maintained at 100-120 ° C until the solution no longer absorbs the hydrogen bromide. The bromide was stratified, washed with organic and concentrated sulfuric acid. The bromide removed from the acid was mixed with 90% methanol of the same volume, washed with ammonia to make the bromide alkaline, washed with 90% methanol and dried with anhydrous calcium chloride. Finally, vacuum distillation, collection of 209-211℃ (1.33kPa) fraction is the finished product, the yield of 90%.
China
