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Vinylphosphonic acid

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1746-03-8 Basic informationMore
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This fireproofing agent, and ingredient for making polymers, is obtained as a syrup on hydrolyzing vinylphosphonyl dichloride with cold H2O and solidifies on prolonged drying over P2O5/KOH. When distilled at 235-240o/0.0006mm, it gives the anhydride (d 1.304, n 1.5874) [Kabachnik & Medvedi Izvest Akad Nauk SSSR, Ser Khim 868 1953, Chem Abstr 54 10834 1960]. It is best kept as the sodium salt (m 350o) which precipitates when a solution of EtOH containing NaOEt (from 2g of Na) is added to vinylphosphonic acid (3.2g), and is recrystallised from EtOH (5.1g, quantitative). The p-anisidinium salt forms mauve prisms m 250o (from EtOH/Et2O). The dimethyl ester, M 136.1, d4 1.1405, nD 1.4330, has b 72.5o/10mm and 197-202o/760mm. [Kabachnik et al. J Gen Chem USSR (Engl Trans) 33 375 1963, Beilstein 4 IV 3568.]
Lastest Price from Vinylphosphonic acid manufacturers
  • Vinylphosphonic acid
  • US $40.00-12.00/kg
  • CAS:1746-03-8
  • Min. Order: 1kg
  • Purity: 0.99
  • Supply Ability: 6 tons
  • 2023-12-11
  • Vinylphosphonic acid
  • US $0.00 /KG
  • CAS:1746-03-8
  • Min. Order: 1KG
  • Purity: 99%
  • Supply Ability: 50000KG/month
  • 2023-08-18

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  • Company Name:Shanghai Thoreco Novel Material Co. Ltd
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    CAS:1746-03-8
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