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Phenoxazine

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USE
Crystallise phenoxazine from EtOH and sublime it in vacuo. If too impure then extract it in a Soxhlet extractor using toluene. Evaporate the solvent and dissolve the residue (ca 100g) in *C6H6 (1L), CARCINOGEN (use an efficient fume cupboard) and chromatograph it through an Al2O3 column (50 x 450 mm) using *C6H6. The eluent (ca 3L) is evaporated to ca 150mL and cooled when ca 103g of phenoxazine m 149-153o is obtained. Sublimation yields platelets m 158-159o. It forms a green picrate m 141.5-142o. [Gilman & Moore J Am Chem Soc 79 3485 1957, Müller et al. J Org Chem 24 37 1959, Beilstein 27 I 223, 27 III/IV 1209.]
Lastest Price from Phenoxazine manufacturers
  • Phenoxazine
  • US $50.00-1.00/KG
  • CAS:135-67-1
  • Min. Order: 1KG
  • Purity: 99%
  • Supply Ability: g-kg-tons, free sample is available
  • 2024-03-25
  • Phenoxazine
  • US $0.00-0.00/KG
  • CAS:135-67-1
  • Min. Order: 1KG
  • Purity: 0.99
  • Supply Ability: 500kg
  • 2023-07-27

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  • Company Name:Zhengzhou HQ Material Co., Ltd.
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