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RUBIJERVINE

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Rubijervine crystallises from 95% EtOH as colourless rods. It has solvent of crystallisation and is dried at 120o/2mm. It is precipitated by digitonin. The hydrobromide crystallises from MeOH/Me2CO with m 265-270o(dec). The diacetate crystallises from MeOH with m 160-163o. The 3-benzoate gives colourless prisms from *C6H6 with m 156-159o and [] D 27.5 +22o (c 1.6, CHCl3). [Pelletier & Locke J Am Chem Soc 79 4531 1957, Jacobs & Craig J Biol Chem 148 41 1943, Beilstein 21 III/IV 2310.]

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